Conservation and Restoration of Cultural Heritage / Kültür Varlıklarını Koruma ve Onarım
Permanent URI for this collectionhttps://hdl.handle.net/11147/23
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Article Citation - Scopus: 1Characteristics and Production Technologies of Byzantine Building Bricks From the Anaia Church in Western Anatolia(Springer, 2023) Çam, Elif; Uğurlu Sağın, ElifFired bricks were valued as essential building materials in the central tradition of Byzantine architecture in Constantinople (Istanbul), Anatolia, and the Balkans. In this study, Byzantine bricks from three construction periods, covering nearly nine centuries (fifth-fourteenth centuries), of Anaia Church (Kadikalesi) in Western Anatolia were investigated to determine their characteristics, raw material properties, and production technologies. The characteristics of the bricks were evaluated and compared in order to identify similarities and differences between the periods and to investigate the continuity of the tradition of brick production over centuries. Basic physical and colorimetric properties, chemical and mineralogical compositions, thermal behavior, and microstructural and mechanical properties of bricks were determined by scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (SEM-EDS), Fourier-transform infrared spectrometry (FTIR), X-ray diffraction (XRD), thermogravimetric analysis (TGA), and mechanical tests. The results indicated that all the bricks in the Anaia Church were brown-beige colored, highly porous, low-density materials with low mechanical strength. They were produced from Ca-rich clays, probably obtained from two different sources used during all construction periods. The mineralogical composition and thermal properties revealed that the bricks from the first and second periods were fired at between 800 and 900 & DEG;C and the bricks from the third period were fired at < 850 & DEG;C. Greater calcium content and firing temperatures were found to reduce the total porosity and the number of small pores (< 10 & mu;m) and increase the mechanical strength of the bricks. The results of the study revealed no significant differences in the production of bricks, including raw material sources and kiln conditions, for the different construction periods of the church.Article Citation - WoS: 27Citation - Scopus: 28Lime Mortar Technology in Ancient Eastern Roman Provinces(Elsevier, 2021) Uğurlu Sağın, Elif; Duran, Hasan Engin; Böke, HasanNatural pozzolanic aggregates were discovered during the Roman era and have been widely used in hydraulic mortar production. Despite the claims of ancient treatises, the properties of pozzolans and the technology of hydraulic lime mortars were well known and applied in the eastern provinces of the Roman Empire. In this study, the characteristics of lime mortar at the ancient sites of Aigai and Nysa located in Western Anatolia were investigated to elicit the technology applied. The raw material compositions of the mortars, the hydraulic properties of the binders, and the mineralogical and chemical compositions of the natural pozzolans used were determined via X-ray diffraction, X-ray fluorescence spectroscopy, scanning electron microscopy coupled with energy dispersive spectroscopy, and thermogravimetric analysis. The major and trace element compositions of the natural pozzolans were evaluated via multivariate statistical analysis to determine whether the same local raw material resources were used in their manufacture. The analytical results indicated that the Roman mortars were hydraulic, stiff, and durable materials due to the use of natural pozzolanic aggregates mostly comprising dacite. Although the aggregates had similar mineralogical compositions, multivariate statistical analysis revealed that their chemical compositions were clearly distinguishable, indicating the use of different sources of raw materials. Thus, it was inferred that similar pozzolan resources were known and deliberately used to produce hydraulic mortars in the eastern ancient Roman provinces.