Conservation and Restoration of Cultural Heritage / Kültür Varlıklarını Koruma ve Onarım
Permanent URI for this collectionhttps://hdl.handle.net/11147/23
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Article Citation - WoS: 21Citation - Scopus: 23Determination of Caco 3 and Sio 2 Content in the Binders of Historic Lime Mortars(Springer Verlag, 2012) Uğurlu Sağın, Elif; Böke, Hasan; Aras, Nadir; Yalçın, ŞerifeThe binders of historic mortars composed of small grain sized silica (SiO 2) and carbonated lime (CaCO 3) are considered as the main part that give hydraulic character and high strength to the mortar. In this study, FTIR, SEM-EDS, LIBS and XRD spectroscopy were used to find out the weight ratios of CaCO 3 to SiO 2 in the binders of historic lime mortars. For this purpose, a series of pure calcium carbonate and silica mixture were prepared in ten combinations in varying ratios from 0.5 to 5. Calibration curve was prepared for each analysis by plotting the peak area or intensity ratios of CaCO 3 to SiO 2 versus the weight ratios of CaCO 3 to SiO 2. A good linear correlation coefficient was obtained for each analysis respectively. The analyses were then tested on the binder of the Roman mortar samples. The results indicated that FTIR, SEM-EDS and LIBS spectroscopy are convenient tools to determine the weight ratios of CaCO 3 to SiO 2 in the binders of mortars. But XRD spectroscopy is not convenient for quantitative analysis of binders due to the presence of varied amounts of amorphous or poor crystalline silica in their compositions.Article Citation - WoS: 28Citation - Scopus: 29Characteristics of Bricks Used in the Domes of Some Historic Bath Buildings(Elsevier Ltd., 2013) Uğurlu Sağın, Elif; Böke, HasanIn this study, characteristics of bricks used in the domes of some historic bath buildings dated to 15th century in Izmir were determined in order to indicate the properties of repair bricks that will be used in the conservation works of the domes. For this purpose, their basic physical properties, elemental and mineralogical compositions, firing temperatures and microstructural properties were determined by using XRF, XRD, SEM-EDS and TGA analysis. Analysis results indicated that the bricks are of low density, high porosity and were produced from raw materials containing low amounts of calcium poor clays fired at low temperatures (<. 900. °C). They are mainly consisted of small pores with r<. 5. μm that make the bricks more susceptible to salt crystallization and freeze-thaw cycles. Although the bricks were fired at low temperatures and susceptible to salt crystallization and freeze thaw cycles, the structural systems of the domes remained without losing their integrity due to the moderate climatic conditions of Izmir. Repair bricks that will be used in the conservation works of the domes should be compatible with the original ones and produced from calcium poor clays by firing at low temperatures.