Mechanical Engineering / Makina Mühendisliği
Permanent URI for this collectionhttps://hdl.handle.net/11147/4129
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Article Citation - WoS: 7Citation - Scopus: 7Investigating the Effects of Pa66 Electrospun Nanofibers Layered Within an Adhesive Composite Joint Fabricated Under Autoclave Curing(American Chemical Society, 2023) Esenoğlu, Gözde; Tanoğlu, Metin; Barışık, Murat; İplikçi, Hande; Yeke, Melisa; Nuhoğlu, Kaan; Türkdoğan, Ceren; Martin, Seçkin; Aktaş, Engin; Dehneliler, Serkan; Gürbüz, Ahmet Ayberk; İriş, Mehmet ErdemEnhancing the performance of adhesively joined composite components is crucial for various industrial applications. In this study, polyamide 66 (PA66) nanofibers produced by electrospinning were coated on unidirectional carbon/epoxy prepregs to increase the bond strength of the composites. Carbon/epoxy prepregs with/without PA66 nanofiber coating on the bonding region were fabricated using the autoclave, which is often used in the aerospace industry. The single lap shear Charpy impact energy and Mode-I fracture toughness tests were employed to examine the effects of PA66 nanofibers on the mechanical properties of the joint region. Scanning electron microscopy (SEM) was used to investigate the nanofiber morphology and fracture modes. The thermal characteristics of Polyamide 66 nanofibers were explored by using differential scanning calorimetry (DSC). We observed that the electrospun PA66 nanofiber coating on the prepreg surfaces substantially improves the joint strength. Results revealed that the single lap shear and Charpy impact strength values of the composite joint are increased by about 79 and 24%, respectively, by coating PA66 nanofibers onto the joining region. The results also showed that by coating PA66 nanofibers, the Mode-I fracture toughness value was improved by about 107% while the glass transition temperature remained constant.Article Citation - WoS: 9Citation - Scopus: 13Analysis of Adhesively Bonded Joints of Laser Surface Treated Composite Primary Components of Aircraft Structures(Elsevier, 2023) Martin, Seçkin; Nuhoğlu, Kaan; Aktaş, Engin; Tanoğlu, Metin; İplikçi, Hande; Barışık, Murat; Yeke, Melisa; Türkdoğan, Ceren; Esenoğlu, Gözde; Dehneliler, SerkanThe performance of the adhesively bonded aerospace structures highly depends on the adhesion strength between the adhesive and adherents, which is affected by, in particular, the condition of the bonding surface. Among the various surface treatment methods, as state of the art, laser surface treatment is a suitable option for the CFRP composite structures to enhance the adhesion performance, adjusting the roughness and surface free energy with relatively minimizing the damage to the fibers. The aim of this study is the validation and evaluation of the adhesive bonding behavior of the laser surface-treated CFRP composite structures, using the finite element technique to perform a conservative prediction of the failure load and damage growth. Such objectives were achieved by executing both experimental and numerical analyses of the secondary bonded CFRP parts using a structural adhesive. In this regard, to complement physical experiments by means of numerical simulation, macro-scale 3D FEA of adhesively bonded Single Lap Joint and Skin-Spar Joint specimens has been developed employing the Cohesive Zone Model (CZM) technique in order to simulate bonding behavior in composite structures especially skin-spar relation in the aircraft wing-box.Article Citation - WoS: 15Citation - Scopus: 17Effects of Nanosecond Laser Ablation Parameters on Surface Modification of Carbon Fiber Reinforced Polymer Composites(SAGE Publications, 2023) Martin, Seçkin; İplikçi, Hande; Barışık, Murat; Türkdoğan, Ceren; Yeke, Melisa; Nuhoğlu, Kaan; Esenoğlu, Gözde; Tanoğlu, Metin; Aktaş, Engin; Dehneliler, Serkan; İriş, Mehmet ErdemRemoval of contaminants and top polymer layer from the surface of carbon-fiber-reinforced polymer (CFRP) composites is critical for high-quality adhesive-joining with direct bonding to the reinforcing fiber constituents. Surface treatment with a laser beam provides selective removal of the polymer matrix without damaging the fibers and increasing the wettability. However, inhomogeneous thermal properties of CFRP make control of laser ablation difficult as the laser energy absorbed by the carbon fibers is converted into heat and transmitted through the fiber structures during the laser operation. In this study, the effect of scanning speed and laser power on nanosecond laser surface treatment was characterized by scanning electron microscope images and wetting angle measurements. Low scanning speeds allowed laser energy to be conducted as thermal energy through the fibers, which resulted in less epoxy matrix removal and substantial thermal damage. Low laser power partially degraded the epoxy the surface while the high power damaged the carbon fibers. For the studied CFRP specimens consisting of unidirectional [45/0/?45/90]2s stacking of carbon/epoxy prepregs (HexPly®-M91), 100 mJ/mm2 generated by 10 m/s scanning speed and 30 W power appeared as optimum processing parameters for the complete removal of epoxy matrix from the top surface with mostly undamaged carbon fibers and super hydrophilic surface condition. © The Author(s) 2023.Research Project Biyobenzetilmis nano yüzey yapıları kullanarak ıslanma ve akış kontrolü(2020) Barışık, MuratProjemizin amacı nano-ölçek yüzey yapılandırmanın yüzey ıslanmasına, akısa ve ısı transferine olan etkilerinin incelenmesidir. Bu nano-ölçek mekanizmaları moleküler dinamik yöntemi ile simüle ettik. Silika-su arasındaki gerekli parametreleri quantum hesapları ile bulduk. Standart yogunluk-fonksiyonları kabüllerinin hesaplayamadıgı fakat dispersive vander- Waals kuvvetlerinin dogru bulunması için gerekli uzun erimli elektron etkilesimlerini DFTD3 grubundan Becke-Johnson modeliyle hesapladık. Devamında silikon yüzeylerin kristal yapısı ve amorf özelliklerine göre ıslanmasındaki degisimini karakterize ettik. Farklı katı yüzey molekül yogunluklarında farklı silikon kristal yapıları seçerken, benzer yüzey molekül yogunlugu aralıgında amorf silikon yapılarını farklı sok sogutmalar yaparak elde ettik. Katı moleküler dizilimlerin ıslanmaya etkisini karakterize ettik. Devamında silika yüzeylerin ıslanmasını inceledik. ?-kristobalit formunun, amorf-silika özelliklerine benzerligi dogrultusunda seçtik. Farklı yüzey yapıları olusturarak ıslanmada olusan degisimi inceledik. Mevcut Cassie-Baxter ve Wenzel ıslatma modellerinin, bu nano-ölçek ıslatma mekanizmalarını tahmin edemedigini gösterdik. Islanma açısının yüzey yapısının geometrik özellikleri ile degisimini karakterize ettik. Devamında yüzey yapılarının neden oldugu çivilenme/takılma etkilerinin literatürde ilk defa detaylı karakterize ettik. Temas çizgisi çıkıntıya takılmıs bir damlacıgın ıslatma açısı damlacık hacminin büyümesi/küçülmesi ile dogrusal oranda artıp/azaldıgını ve bu davranısın boyutlardan ve yüzey ıslatma özelliklerinden bagımsız olarak yüzey yapısının ve damlacıgın büyüklüklerinin oranı cinsinden olustugunu gösterdik. Devamında çalısdıgımız degisik yapılara sahip yüzeylerden nano-kanallar olusturduk. Bu kanallarda basınçla sürülen akısların hız profillerini ve arayüzlerinde olusan kayma hızlarını ölçtük. Yüzey yapılarının ıslanma açısını arttırarak yüzeyi hydrophobik yapmasına ragmen beklenenin aksine kayma hızını azalttıgını bulduk. Mevcut literatürde ıslanma açısının artmasıyla kayma uzunlugu artısını açıklayan modellerin düz olmayan yüzeylerde geçerli olmadıgını gösterdik. Devamında aynı kanal setinde duvardan duvara tek yönde iletim ile ısı transferi çalıstık. Sıcaklık profillerinden arayüz ısıl direnci nedeniyle olusan sıcaklık atlamalarını Kapitza uzunlugu cinsinden ölçtük. Kapitzanın da artan ıslanma açısına karsın azaldıgını gösterdik. Sonuçta ıslanma açısını, kayma hızını ve Kapitza uzunlugunu yüzey yapısının hacmi, yüksekligi ve genisligi cinsinden karakterize ettik. Ihtiyaç duyulan ıslanma, akıs yada ısı transferi yüzey yapılarıyla ayarlanabilir.Article Citation - WoS: 8Citation - Scopus: 8Improving Adhesive Behavior of Fiber Reinforced Composites by Incorporating Electrospun Polyamide-6,6 Nanofibers in Joining Region(SAGE Publications, 2022) Esenoğlu, Gözde; Barışık, Murat; Tanoğlu, Metin; Yeke, Melisa; Türkdoğan, Ceren; İplikçi, Hande; Martin, Seçkin; Nuhoğlu, Kaan; Aktaş, Engin; Dehneliler, Serkan; İriş, Mehmet ErdemAdhesive joining of fiber reinforced polymer (CFRP) composite components is demanded in various industrial applications. However, the joining locations frequently suffer from adhesive bond failure between adhesive and adherent. The aim of the present study is improving bonding behavior of adhesive joints by electrospun nanofiber coatings on the prepreg surfaces that have been used for composite manufacturing. Secondary bonding of woven and unidirectional CFRP parts was selected since this configuration is preferred commonly in aerospace practices. The optimum nanofiber coating with a low average fiber diameter and areal weight density is succeed by studying various solution concentrations and spinning durations of the polyamide-6.6 (PA 66) electrospinning. We obtained homogeneous and beadles nanofiber productions. As a result, an average diameter of 36.50 +/- 12 nm electrospun nanofibers were obtained and coated onto the prepreg surfaces. Prepreg systems with/without PA 66 nanofibers were hot pressed to fabricate the CFRP composite laminates. The single-lap shear test coupons were prepared from the fabricated laminates to examine the effects of PA 66 nanofibers on the mechanical properties of the joint region of the composites. The single-lap shear test results showed that the bonding strength is improved by about 40% with minimal adhesive use due to the presence of the electrospun nanofibers within the joint region. The optical and SEM images of fractured surfaces showed that nanofiber-coated joints exhibited a coherent failure while the bare surfaces underwent adhesive failure. The PA66 nanofibers created better coupling between the adhesive and the composite surface by increasing the surface area and roughness. As a result, electrospun nanofibers turned adhesive failure into cohesive and enhanced the adhesion performance composite joints substantially.Article Citation - WoS: 5Citation - Scopus: 6Active Heat Transfer Enhancement by Interface-Localized Liquid Dielectrophoresis Using Interdigitated Electrodes(Elsevier, 2022) Yenigün, Onur; Barışık, MuratWe introduced an active heat transfer control between graphene and water using interdigitated electrodes (IDEs). Oppositely charged co-planer electrodes embedded on a graphene surface created a non-uniform electric field. Resulted interface localized liquid dielectrophoresis (LDEP) perpendicular to surface enhanced the water/graphene coupling and decreased interfacial thermal resistance (ITR) substantially. We correlated the theoretical calculations of average electric field strength near surface with Kapitza values measured at corresponding electrode configurations. We obtained a unified linear variation of Kapitza as a function of average electric strength independent of electrode size and charge. By increasing the electric field strength, we measured up to 96% decrease of Kapitza near electrodes. Since the IDEs generated electric field was only interface localized, it required lower electrode charges than any parallel-plate capacitor systems. We showed that ITR remains effective in heat transfer behavior for systems as big as 100nm such that interface localized electric field can at least increase the heat removal 50% by eliminating the ITR from both graphene/water interfaces of a channel system. By converting hydrophobic few-layer graphene to super-hydrophilic condition with ultra-low Kapitza, current results are important for graphene-based materials considered for the solution of the thermal management problem of current and next generation micro/nano-electronics.Article Citation - WoS: 16Citation - Scopus: 17Thermal and Hydrodynamic Behavior of Forced Convection Gaseous Slip Flow in a Kelvin Cell Metal Foam(Elsevier, 2022) Sabet, Safa; Barışık, Murat; Buonomo, Bernardo; Manca, OronzioPorous metallic foams are a key material in numerous thermal and hydraulic applications. Gas flows in such micro/nanoporous systems deviate from classical continuum descriptions due to nonequilibrium in gas dynamics, and the resulted heat and mass transport show variation by rarefaction. This study performed a wide range of pore-level analysis of convective gas flows in a Kelvin cell model at different porosities and working conditions. Rarefaction effects onto permeability and heat transfer coefficients were calculated through Darcy to Forchheimer flow regimes. Permeability increased up to 60% by increasing rarefaction while this enhancement decreased by increasing porosity. At the same time, rarefaction lessened inertial effects such that Forchheimer coefficients decreased substantially. At high flow velocities, the increase in rarefaction considerably decreased the effect of drag forces. Hence, hydrodynamic enhancement due to rarefaction was found to increase by increasing Reynolds number. On the other hand, positive influence of boundary slip and negative influence of temperature jump developing between gas and solid almost canceled each other for the studied low heat flux region of highly conductive metal foam structures. Hence, Nusselt numbers were found mostly related to Reynolds number independent from rarefaction. We described Nusselt value based on power law model as a function of Reynolds and porosity. Results and the proposed model are important to accurately predict the thermal and hydrodynamic performance of metal foams in the 80 PPI range.Article Citation - WoS: 7Citation - Scopus: 8Size and Roughness Dependent Temperature Effects on Surface Charge of Silica Nanoparticles(Elsevier, 2021) Alan, Büşra Öykü; Barışık, MuratSilica nanoparticles (SNP) with different sizes and surface areas are used in numerous micro/nanofluidic applications, while their surface charge properties play a major role in their function. In many of these applications, SNPs also undergo temperature variation. We present that an increase in temperature yields a substantial increase in SNP surface charge depending on nanoparticle size and surface roughness, which cannot be estimated by existing theory. As a continuation of our earlier work characterizing the deviation of SNP surface charging from theoretical predictions due to curvature and EDL overlap effects, this study presents the differentiation from the theory in temperature dependence under various conditions. As we calculate surface chemistry as a function of local ionic conditions (Charge Regulation), temperature variation changed the equilibrium constants of protonation/deprotonation reactions of the SNP surface, in addition to changes occurring in relative permittivity and ionic mobilities. Results show that variation of SNP surface charge by temperature decreases by decreasing particle size and/or increasing roughness size, compare to theoretical flat plate calculations considering similar temperature-dependent properties and charge regulation on the surface. We characterized these deviations by obtaining an electrokinetic similarity between different systems of various size and roughness at various ionic conditions based on the non-dimensional groups of lambda/DP and lambda/DR. Based on these, we devised a phenomenological model as an extension to the flat plate theory to successfully predict the surface charge of SNPs as a function of the particle size, roughness size, and temperature. The current findings are important for the characterization of SNPs through temperature variations and can also be used to adjust the surface charge of SNPs by tuning the temperature.Article Citation - WoS: 22Citation - Scopus: 24Size Dependent Influence of Contact Line Pinning on Wetting of Nano-textured/Patterned Silica Surfaces(Royal Society of Chemistry, 2020) Özçelik, H. Gökberk; Satıroğlu, Ezgi; Barışık, MuratWetting behavior on a heterogeneous surface undergoes contact angle hysteresis as the droplet stabilized at a metastable state with a contact angle significantly different from its equilibrium value due to contact line pinning. However, there is a lack of consensus on how to calculate the influence of pinning forces. In general, the pinning effect can be characterized as (i) microscopic behavior when a droplet is pinned and the contact angle increases/decreases as the droplet volume increases/decreases and (ii) macroscopic behavior as the pinning effects decrease and ultimately, disappear with the increase of the droplet size. The current work studied both behaviors using molecular dynamics (MD) simulation with more than 300 different size water droplets on silica surfaces with three different patterns across two different wetting conditions. Results showed that the contact angle increases linearly with increasing droplet volume through the microscopic behavior, while the droplet is pinned on top of a certain number of patterns. When we normalized the droplet size with the corresponding pattern size, we observed a "wetting similarity" that linear microscopic contact angle variations over different size heterogeneities continuously line up. This shows that the pinning force remains constant and the resulting pinning effects are scalable by the size ratio between the droplet and pattern, independent of the size-scale. The slope of these microscopic linear variations decreases with an increase in the droplet size as observed through the macroscopic behavior. We further found a universal behavior in the variation of the corresponding pinning forces, independent of the wetting condition. In macroscopic behavior, pinning effects become negligible and the contact angle reaches the equilibrium value of the corresponding surface when the diameter of the free-standing droplet is approximately equal to 24 times the size of the surface structure. We found that the pinning effect is scalable with the droplet volume, not the size of the droplet base.Article Citation - WoS: 9Citation - Scopus: 13Local Heat Transfer Control Using Liquid Dielectrophoresis at Graphene/Water Interfaces(Elsevier Ltd., 2021) Yenigün, Onur; Barışık, MuratGraphene-based materials are considered for the solution of the thermal management problem of current and next generation micro/nano-electronics with high heat generation densities. However, the hydrophobic nature of few-layer graphene makes passing heat to a fluid very challenging. We introduced an active and local manipulation of heat transfer between graphene and water using an applied, non-uniform electric field. When water undergoes electric field induced orientation polarization and liquid dielectrophoresis, a substantial increase in heat transfer develops due to a decrease in interfacial thermal resistance and increase in thermal conductivity. By using two locally embedded pin and plate electrodes of different sizes, we demonstrated a two-dimensional heat transfer control between two parallel few-layer graphene slabs. We obtained local heat transfer increase up to nine times at pin electrode region with an ultra-low Kapitza resistance through the studied non-uniform electric field strength range creating highly-ordered compressed water in the experimentally measured density limits. With this technique, heat can be (i) distributed from a smaller location to a larger section and/or (ii) collected to a smaller section from a larger region. Current results are important for hot spot cooling and/or heat focusing applications. © 2020