Mechanical Engineering / Makina Mühendisliği
Permanent URI for this collectionhttps://hdl.handle.net/11147/4129
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Research Project Üstüniletken MgB2 tellerin üretimi ve karakterizasyonu(TÜBİTAK - Türkiye Bilimsel ve Teknolojik Araştırma Kurumu, 2005) Okur, Salih; Özyüzer, Lütfi; Abukay, Doğan; Emirdağ, Mehtap; Tanoğlu, Metin; Eğilmez, MehmetMgB2 alaşımının 39 K lik Tc kritik sıcaklığına sahip bir üstüniletken olduğunun 2001 de keşfedilmesi çok iyi üstüniletken olduğu bilinen NbTi ve NbsSn malzemelerinin yanısıra uygulamaya daha yakın yeni bir üstüniletken malzeme olma ümidini de artırmıştır. O günden bu güne MgB2 üstüniletken tellerin üretilmesi konusunda çok etkileyici bir aşama kaydedilmiştir. Daha yüksek kritik akım yoğunluğuna ulaşmak için gerekli parametrelerin araştırılması konusunda birkaç teknik geliştirilmiştir. Bunların arasında 'tüp içinde toz ' (TIT) adı verilen metot diğerlerine göre daha pratik ve ümit verici gözükmektedir. Bazı metal ve alaşımların TIT işleminde kılıf malzeme olarak kullanılmaya uygun bulunmuştur. Bunlardan demir ve alaşımları kısmen MgB2 özelliğini bozmadığı gibi manyetik ekranlama yaparak dış manyetik alanların kritik akım üzerindeki yan etkilerini azaltarak daha yüksek değerlere ulaşılmıştır. TIT yöntemi ile MgB2 üretimi sırasında iki farklı teknik vardır. Birisinde reaktif MgB2 tozlar kulanılırken diğerinde belli kimyasal oranlarda karıştırılmış reaktif olmayan Mg+2B tozları kullanılmaktadır. Daha sonra bu tozlar reaksiyon yapmayan bir tüp veya kapsül içine kapatılıp 900 ile 1000 °C civarında belirli bir süre tavlanmaktadır. Bu yöntem ile Demir kılıflı MgB2 üstüniletken tellerinden 15 K de 10 A/cm civarında bir Jc kritik akım yoğunluğuna ulaşılmıştır. Bu projede ilk adım olarak borik asitten M&B2 elde edilmiş ve elde edilen MgB2 in yapısını XRD ve SEM EDX mikroskopu ile karakterize edilmiştir. Uygun bir saflığa sahip MgB2 e ulaşıldığında elektriksel ve manyetik özellikleri pellet haline getirilip incelenmiştir, ikinci adımda ise üretilen MgB2 tozlarından üstüniletken MgB2 tel ve teyplerin TIT yöntemi ile üretilmiştir ve Cu, Fe, ve paslanmaz çelik gibi MgB2 ile etkileşmeyen malzemeler kılıf olarak kullanılanarak üretilmeye çalışılmış ve bu üstüniletken MgB2 tellerin özdirenç ve manyetik alana bağlı olarak kritik akım (Jc) karakteristiğinin sıcaklığa bağımlılığı incelenmiştir.Research Project Üstüniletken magnezyum borür (MgB2) tellerinin yüksek akım ve yüksek manyetik alan uygulamaları için geliştirilmesi(2008) Okur, Salih; Tarhan, Enver; Büyükköse, Serkan; Özyüzer, Lütfi; Tanoğlu, Metin; Emirdağ, Mehtap[No Abstract Available]Research Project Nanokompozit malzemelerin polimer ve tabakalı kil yapılardan geliştirilmesi ve karakterizasyonu(2009) Tanoğlu, Metin; Okur, Salih[No Abstract Available]Article Citation - WoS: 15Citation - Scopus: 14Development of Electrically Conductive and Anisotropic Gel-Coat Systems Using Cnts(Elsevier Ltd., 2013) İnce Yardımcı, Atike; Tanoğlu, Metin; Selamet, YusufElectrical conductivity of an unsaturated thermoset polyester based gel-coat system containing 0.05 wt.% of carbon nanotubes (CNTs) was investigated. The CNTs used were synthesized by chemical vapor deposition method by methane decomposition and Raman characterization showed that they were mostly single walled and high quality. To disperse CNTs in the gel-coat resin, 3-roll milling technique was used. It was found that as the CNTs are added to gel-coat system, resistivity value decreases significantly while neat gel-coat showed a high resistivity. By the application of an AC electrical field during curing process, it was attempted to align CNTs in the gel-coat resin and an electrically anisotropic polymer was obtained. © 2012 Elsevier B.V. All rights reserved.Article Citation - WoS: 8Citation - Scopus: 12A Microstructural Study of Surface Hydration on a Magnesia Refractory(Elsevier Ltd., 2010) Sütçü, Mücahit; Akkurt, Sedat; Okur, SalihHydration of the surface of a periclase refractory was studied in a controlled humidity atmosphere (92% relative humidity) at 26 °C for up to 92 h. The effect of humidity on the specimens was examined using a scanning probe microscope (SPM) and a scanning electron microscope (SEM), which showed that the degree of hydration was noticeably less in the intergranular bond phase compared to the periclase crystallites. The SPM study indicated significant growth of hydrates on the refractory grain surface. Growth rate of the hydrate layer was least on (0 0 1) orientation, higher for the (1 0 3) orientation, and highest for the (1 0 1) oriented grain. The rate of loss of refractory phases by hydration on a (1 0 1) oriented grain was 4.53 nm/h. This material loss may be insignificant for a bulk brick, but is a serious threat for a magnesia castable consisting of fine magnesia powder due to large surface area exposed to humidity or water itself. © 2010 Elsevier Ltd and Techna Group S.r.l. All rights reserved.Article Citation - WoS: 15Citation - Scopus: 17Influence of Crystallographic Orientation on Hydration of Mgo Single Crystals(Elsevier Ltd., 2009) Sütçü, Mücahit; Akkurt, Sedat; Okur, SalihThis study has been performed in order to find out the influence of crystallographic orientation on hydration of MgO single crystal substrates with (1 0 0)-, (1 1 0)-, and (1 1 1)-orientations. The samples were left in a hydration chamber with an 88% relative humidity for 18 h at room temperature. The effect of humidity on the samples was examined by scanning probe microscope (SPM) and scanning electron microscope (SEM) which showed that the degree of hydration was noticeably influenced by the crystallographic orientation. It was found that the MgO with (1 1 1)-orientation has the highest tendency to hydrate than the other orientations. Second most affected sample was (1 1 0) crystal. Loss of MgO on the surface by hydration is most severe when the crystal is oriented in (1 1 1) plane with the maximum hydrate layer thickness of 174 nm after 18 h of exposure.Article Citation - WoS: 38Citation - Scopus: 42Layered Clay/Epoxy Nanocomposites: Thermomechanical, Flame Retardancy, and Optical Properties(John Wiley and Sons Inc., 2008) Kaya, Elçin; Tanoğlu, Metin; Okur, SalihIn this study, layered clay/polymer nano-composites were developed based on epoxy resins and montmorillonite as the nanoplatelet reinforcement. Clay particles were treated with hexadecyltrimethylammonium chloride (HTCA) through an ion exchange reaction. In this way, Na+ interlay er cations of the clay is exchanged with onium cation of the surfactant that turns the hydrophilic clays (MMT) to organophilic (OMMT) characteristics. Thermal analysis results revealed that the glass transition temperature (Tg) and the dynamic mechanical properties including the storage and loss modulus of the neat epoxy resin increases by the incorporation of clay particles. It was also found that flame resistance of the polymer is improved by the addition of the clay particles.Article Citation - WoS: 3Citation - Scopus: 3Thermostable Tensoresistors of Co Doped Gasb-Fega1.3 Eutectic Composites(Elsevier Ltd., 2008) Rahimov, R. N.; Khalilova, A. A.; Arasly, D. H.; Aliyev, M. I.; Tanoğlu, Metin; Özyüzer, LütfiThe microstructure and tensoresistive properties of GaSb-FeGa1.3 eutectic composites doped with 0.1% Co have been investigated. It was found that the Co impurity atoms mainly accumulate in the metallic inclusions. The length of the inclusions in GaSb-FeGa1.3〈Co〉 was measured to be about half of those in undoped GaSb-FeGa1.3 eutectics. The tensometric characteristics of gauges based on GaSb-FeGa1.3〈Co〉 have been found to be more thermostable than undoped samples. © 2008 Elsevier B.V. All rights reserved.Article Citation - WoS: 6Citation - Scopus: 11Electrical and Mechanical Properties of Superconducting Mgb2/Mg Metal Matrix Composites(IOP Publishing Ltd., 2006) Eğilmez, Mehmet; Özyüzer, Lütfi; Tanoğlu, Metin; Okur, Salih; Kamer, Orhan; Öner, YıldırhanMgB2/Mg composites were prepared using a metal matrix composite fabrication method that offers the potential to produce superconducting wires as an alternative approach to the powder in tube process. To obtain composites, MgB2 and Mg powders were mixed at different weight fractions and uniaxially pressed in a cylindrical die under the pressure of 0.5 and 1.0GPa for two hours at various temperatures. The x-ray diffraction technique was used for phase identification. Temperature dependence of resistivity and magnetization measurements were carried out to determine superconducting properties. The effects of composite fabrication temperature and the addition of the Mg on the mechanical properties of MgB2/Mg composites were investigated. For this purpose, the compressive mechanical testing was performed to measure the elastic modulus and fracture strength values of the composites. It was found that the relative weight fraction of the Mg and the fabrication conditions of the composites have considerable effect on the superconducting and mechanical properties of the composites.Article Citation - WoS: 13Citation - Scopus: 12Mgb2 Superconducting Thin Films Sequentially Fabricated Using Dc Magnetron Sputtering and Thermionic Vacuum Arc Method(Elsevier Ltd., 2007) Okur, Salih; Kalkancı, M.; Pat, Suat; Ekem, Naci; Akan, Tamer; Balbağ, Zafer; Musa, G.; Tanoğlu, MetinIn this work, we discuss fabrication and characterization of MgB2 thin films obtained by sequential deposition and annealing of sandwich like Mg/B/Mg thin films on glass substrates. Mg and B films were prepared using DC magnetron sputtering and thermionic vacuum arc techniques, respectively. The MgB2 thin films showed superconducting critical transition at 33 K after annealing at 650 °C.