Mechanical Engineering / Makina Mühendisliği
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Article Citation - WoS: 54Citation - Scopus: 58Sintering and Microstructural Investigation of Gamma–alpha Alumina Powders(Elsevier Ltd., 2014) Yalamaç, Emre; Trapani, Antonio; Akkurt, SedatSintering behaviors of commercially available alumina powders were investigated using constant-heating rate dilatometric experiments. Each powder had different proportion of alpha/gamma alumina. Densification behaviors of powders were studied up to 1600 °C with three different heating rates of 1, 3.3 and 6.6 °C/min. Compacts of different gamma content alumina powders exhibited systematic anomalous second peaks in the densification rate curves at certain heating rates and temperatures. At 3.3 °C/min heating rate experiments, densification curves of 10% gamma phase alumina powder compacts reached a plateau after 1450 °C, and did not increase any further at higher temperatures. This phenomenon was double checked to understand powder behavior during sintering. 10% gamma phase alumina powder compacts showed the highest density for each heating rate. It reached 94% theoretical density with 1 °C/min heating rate. But 20% gamma phase alumina powder compacts had the finest grain size of about 1.40 ?m. Final density and porosity of compacts were also tested by image analysis and the results were coherent with Archimedes results. © 2014 Karabuk UniversityArticle Citation - WoS: 171Characteristics of Brick Used as Aggregate in Historic Brick-Lime Mortars and Plasters(Elsevier Ltd., 2006) Böke, Hasan; Akkurt, Sedat; İpekoğlu, Başak; Uğurlu, ElifMortars and plasters composed of a mixture of brick powder and lime have been used since ancient times due to their hydraulic properties. In this study, raw material compositions, basic physical, mineralogical, microstructural and hydraulic properties of some historic Ottoman Bath brick-lime mortars and plasters were determined by XRD, SEM-EDS, AFM, TGA and chemical analyses. The mineralogical and chemical compositions, microstructures, morphologies and pozzolanicities of the brick powders and fragments used as aggregates in the mortars and plasters were examined to find out the relationship between hydraulic properties of the mortars and the bricks. The characteristics of bricks used in the bath domes were also determined to investigate whether the brick aggregates used in mortar and plasters were prepared from these bricks. The results indicated that the mortars and plasters were hydraulic owing to the presence of crushed brick powders that have good pozzolanicity. The brick powders bad high pozzolanicity because they contained high amounts of calcium-poor clay minerals in their raw materials that were fired at low temperatures. On the other hand, bricks used in the domes had poor pozzolanicity with different mineralogical and chemical compositions from bricks used in mortars and plasters. Based on the results of the analysis, it was thought that the bricks manufactured with high amounts of clays were consciously chosen in the preparation of hydraulic mortars and plasters. (C) 2006 Elsevier Ltd. All rights reserved.Article Citation - WoS: 25Citation - Scopus: 26Lowering the Sintering Temperature of Solid Oxide Fuel Cell Electrolytes by Infiltration(Elsevier Ltd., 2019) Sındıraç, Can; Çakırlar, Seda; Büyükaksoy, Aligül; Akkurt, SedatA dense electrolyte with a relative density of over 95% is vital to prevent gas leakage and thus the achievement of high open circuit voltage in solid oxide fuel cells (SOFCs). The densification process of ceria based electrolyte requires high temperatures heat treatment (i.e. 1400-1500 degrees C). Thus, the minimum co-sintering temperatures of the anode-electrode bilayers are fixed at these values, resulting in coarse anode microstructures and consequently poor performance. The main purpose of this study is to densify gadolinia doped ceria (GDC), a common SOFC electrolyte, at temperatures lower than 1400 degrees C. By this aim, an approach involving the infiltration of polymeric precursors into porous electrolyte scaffolds, a method commonly used for composite SOFC electrodes, is proposed. By infiltrating polymeric precursors of GDC into porous GDC scaffolds, a reduction in the sintering temperature by at least 200 degrees C is achieved with no additives that might affect the electrical properties. Energy dispersive x-ray spectroscopy line scan analyses performed on porous GDC scaffolds infiltrated by a marker solution (polymeric FeOx precursor in this case) reveals a homogeneous infiltrated phase distribution, demonstrating the effectiveness of polymeric precursors.Article Citation - WoS: 23Citation - Scopus: 24Constructal Branched Micromixers With Enhanced Mixing Efficiency: Slender Design, Sphere Mixing Chamber and Obstacles(Elsevier Ltd., 2019) Çetkin, Erdal; Miguel, Antonio F.Here we uncover the passive micromixer designs with the maximum mixing efficiency under a lesser flow impedance. Three different designs of micromixers were considered for volume constrained systems: branched systems of ducts, branching ducts with sphere mixing chamber and branching ducts with obstacles. The best performing designs, with maximum mixing efficiency and minimum flow impedance, are uncovered numerically by considering three degrees of freedom (ratios between diameters, between lengths, and between length and diameter) under total volume constraint. The mixing efficiency, the flow impedance and the mixer performance (or mixer quality) for all the designs are determined based on numerical results. The results uncover that the branched micromixer should have long mother ducts with larger diameter than daughter ducts. Our results also show that branching ducts with sphere mixing chambers and obstacles also enhance the mixing efficiency but with an additional penalty on flow impedance. Besides, systems with a sphere mixing chamber insertion in the junction between mother and daughter ducts have greater mixing efficiency than systems with embedded obstacles into the mother channel. However, for a given flow impedance, the mixing efficiency is greater for branched systems of ducts than for branching ducts with sphere mixing chamber and with obstacles. For mixer systems built in a space with limited size, branching ducts with sphere mixing chamber may be a good option because they require less space than the other systems. Here new analytical models are also proposed to predict the mixing efficiency and mixer performance based on numerical results. In summary, this paper provides important insights for the designers of micromixer based on Constructal law. (C) 2018 Elsevier Ltd. All rights reserved.Article Citation - WoS: 21Citation - Scopus: 24Effect of Nano-Film Thickness on Thermal Resistance at Water/Silicon Interface(Elsevier Ltd., 2019) Yenigün, Onur; Barışık, MuratParallel to the developments in micro/nano manufacturing techniques, component sizes in micro/nano electro mechanical systems have been decreasing to nanometer scales. Decrease in lengths in heat transfer direction below the heat carrier phonon length scales reduces thermal conduction in semiconductors. This study shows that such altered phonon spectrums with the decrease of size also reduce the heat transfer at the solid/liquid interfaces and can be correlated with the thermal conductivity of the slab. Using Molecular Dynamics (MD), we measured heat transfer between water and silicon of different thickness between 5 nm and 60 nm. Silicon slabs exhibit a linear temperature profile through the bulk where thermal conductivities measured based on Fourier law decreased by the decreasing slab thickness. We applied a semi-theoretical formulism on variation of conductivity by slab thickness. At the interface of these slabs and water, heat passage is disturbed due to the phonon mismatch of dissimilar materials, which is mostly considered as solid/liquid couple interface properties by the earlier literature. Resistance for phonon passage characterized as Kapitza length (L-K) is measured for different slab thicknesses at different surface wetting conditions varying between hydrophilic to hydrophobic. Increasing surface wetting decreases the L-K while at a certain wetting, decreasing the slab thickness increases the L-K. Once the L-K of different size slabs normalized by its bulk value (assumed to be the L-K of the thickest slab at the corresponding wetting), L-K variation by silicon thickness shows a universal behavior independent of surface wetting. A mathematical model describing the exponential increase of L-K by decreasing thickness was developed and validated by an earlier model. We further developed a correlation between the corresponding changes of L-K and conductivity with respective to their bulk values by analytically combining two models as (L-K/L-K-(Bulk)) = exp (3.94(k(Bulk) - k)/(k x k(Bulk))), using which L-K can be predicted from available thermal conductivities of a certain material. Results are crucial for thermal management of current and future electronics. (C) 2019 Elsevier Ltd. All rights reserved.Article Citation - WoS: 11Citation - Scopus: 12Electrical Properties of Gadolinia Doped Ceria Electrolytes Fabricated by Infiltration Aided Sintering(Elsevier Ltd., 2019) Sındıraç, Can; Büyükaksoy, Aligül; Akkurt, SedatCommon solid oxide fuel cell (SOFC) electrolyte materials (e.g., gadolinia doped ceria - GDC) demand temperatures exceeding 1400 degrees C for densification by conventional solid state sintering. It is very desirable to reduce the densification of the SOFC electroltytes to i) avoid microstructural coarsening of the composite anode layers, which are co-sintered with the electolyte layer in the anode supported SOFC fabrication scheme and ii) reduce energy consumption during SOFC manufacturing. We have recently demostrated a novel infiltration-aided sintering route to densify GDC ceramics at 1200 degrees C. In the present work, we present the electrical properties of GDC ceramics fabricated thusly. Comparison of high density (>= 95%) samples fabricated by conventional or infiltration-aided sintering reveal that at 700 degrees C, similar total electrical conductivities are obtained, while at 300 degrees C, specific grain boundary resistivity is smaller in the latter. Bulk (grain) conductivity is higher in porous GDC ceramics (relative density <= 90%) fabricated by infiltration-aided sintering than the conventionally sintered ones with similar porosities. Finally, open circuit voltage of 0.84 V at 700 degrees C, obtained under dilute hydrogen and stagnant air conditions suggests that GDC ceramics densified by infiltration-aided sintering are suitable for use as SOFC electrolytes.Article Citation - WoS: 31Citation - Scopus: 31Snowflake Shaped High-Conductivity Inserts for Heat Transfer Enhancement(Elsevier Ltd., 2018) Konan, Hasel Çiçek; Çetkin, ErdalHere, we show numerically how thermal resistance in a two-dimensional domain with a point heat source can be reduced with embedded high-conductivity snowflake shaped pathways. The external shape of the domain is square, and its boundaries are heat sink. The geometry of the inserted pathways which corresponds to the minimum Tmax was uncovered with the consideration of Constructal Theory, i.e. the constructal design. In the first assembly, number of mother (big) fins was uncovered as the area fraction increases. The results of the first assembly indicate that the increase in number of mother fins does not increase heat transfer after a limit number for the fins. After uncovering the mother pathway geometry corresponding to the minimum Tmax, the daughter (small) fins inserted at the tip of them, i.e. second assembly. In the second assembly, the fin ratios, small fin location and angle were discovered when the area fraction is fixed. In addition, in the third assembly, larger daughter fins were attached to mother fins. The results of the second and third assemblies document what should be the geometric length scales and the number of daughter fins in order to minimize Tmax. The constructal design uncovered is similar to the shape of snowflakes. Therefore, the results also uncover snowflakes correspond to the designs with minimum thermal conductivity, i.e., not mimicking the nature but understanding it with physics.Article Citation - WoS: 19Citation - Scopus: 21Dynamic Crushing Behavior of a Multilayer Thin-Walled Aluminum Corrugated Core: the Effect of Velocity and Imperfection(Elsevier Ltd., 2018) Sarıyaka, Mustafa; Taşdemirci, Alper; Güden, MustafaThe crushing behavior of a multilayer 1050 H14 aluminum corrugated core was investigated both experimentally and numerically (LS-Dyna) using the perfect and imperfect models between 0.0048 and 90 m s−1. The dynamic compression and direct impact tests were performed in a compression type and a modified Split Hopkinson Pressure Bar set-up, respectively. The investigated fully imperfect model of the corrugated core sample represented the homogenous distribution of imperfection, while the two-layer imperfect model the localized imperfection. The corrugated core experimentally deformed by a quasi-static homogenous mode between 0.0048 and 22 m s−1, a transition mode between 22 and 60 m s−1 and a shock mode at 90 m s−1. Numerical results have shown that the stress-time profile and the layer crushing mode of the homogeneous and transition mode were well predicted by the two-layer imperfect model, while the stress-time profile and the layer crushing mode were well approximated by the fully imperfect model. The fully imperfect model resulted in complete sequential layer crushing at 75 and 90 m s−1, respectively. The imperfect layers in the shock mode only affected the distal end stresses, while all models implemented resulted in similar impact end stresses. The distal end initial crushing stress increased with increasing velocity until about 22 m s−1; thereafter, it saturated at ~2 MPa, which was ascribed to the micro inertial effect. Both the stress-time and velocity-time history of the rigid-perfectly-plastic-locking model and the critical velocity for the shock deformation were well predicted when a dynamic plateau stress determined from the distal end stresses in the shock mode was used in the calculations.Article Citation - WoS: 28Citation - Scopus: 28Crushing Behavior and Energy Absorption Performance of a Bio-Inspired Metallic Structure: Experimental and Numerical Study(Elsevier Ltd., 2018) Taşdemirci, Alper; Akbulut, Emine Fulya; Güzel, Erkan; Tüzgel, Fırat; Yücesoy, Atacan; Şahin, Selim; Güden, MustafaA thin-walled structure inspired from a biologic creature known as balanus was investigated experimentally and numerically under quasi-static and dynamic loads for load-carrying and energy absorption properties. The structure was composed of an inner conical core with a hemispherical cap and an outer shell in frusto-conical shape and formed by deep drawing. The applied deep drawing process was modelled using nonlinear finite element code LS-DYNA to determine the residual stress/strain and the non-linear thickness distribution after the forming process. It was also shown that the load carried by the balanus structure was greater than the arithmetic sum of the load carried by the inner core and by the outer shell separately. Although the mean force increase due to interaction effect at quasi-static strain rate was approximately 5%, while it increased to roughly 26% at dynamic strain rates in drop weight experiments. The numerical models also showed that the outer shell absorbed more energy than the inner core while the difference between the energy absorbing performance of the core and shell decreased with increasing deformation rate. The effect of strain rate and inertia on the increase in crush load increased with increasing impact velocity, while the strain rate effect had greater influence than the inertia on the crush load. The increased load carrying capacity of the balanus at quasi-static and dynamic strain rates was ascribed to the interaction between the core and shell and the confinement effect of the outer shell particularly at dynamic strain rate.Article Citation - WoS: 97Citation - Scopus: 110Effect of Polyamide-6,6 (pa 66) Nonwoven Veils on the Mechanical Performance of Carbon Fiber/Epoxy Composites(Elsevier Ltd., 2018) Beylergil, Bertan; Tanoğlu, Metin; Aktaş, EnginIn this study, carbon fiber/epoxy (CF/EP) composites were interleaved with polyamide-6,6 (PA 66) nonwoven veils at two different areal weight densities (17 and 50 gsm) to improve their delamination resistance against Mode-I loading. Mode-I fracture toughness (DCB), tensile, open hole tensile (OHT), flexural, compression, short beam shear (ILSS) and Charpy-impact tests were performed on the reference and PA 66 interleaved composite specimens. The DCB test results showed that the initiation and propagation Mode-I fracture toughness values of the composites were significantly improved by 84 and 171% using PA 66-17 gsm veils respectively, as compared to reference laminates. The use of denser PA 66-50 gsm veils in the interlaminar region led to higher improvement in fracture toughness values (349% for initiation and 718% for propagation) due to the higher amount of veil fibers involved in fiber bridging toughening mechanism. The incorporation of PA 66-50 gsm nonwoven veils also increased the ILSS and Charpy impact strength of the composites by 25 and 15%, respectively. On the other hand, the PA 66 veils reduced in-plane mechanical properties of CF/EP composites due to lower carbon fiber volume fraction and increased thickness.