Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
Permanent URI for this collectionhttps://hdl.handle.net/11147/7148
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Article Microstructure-Based Prediction of Mechanical Properties of Austempered Ductile Iron Using Multiple Linear Regression Analysis(Springer int Publ Ag, 2025) Yalcin, M. Alp; Davut, KemalMultiple linear regression analysis (MLRA) was used to predict the mechanical properties of austempered ductile iron (ADI) including yield and tensile strength, uniform elongation, hardening exponent, as well as fracture energy by building a model that uses characteristic features of microstructural constituents as input parameters. The complex multi-scale microstructure of ADI, which is composed of spherical graphite particles over 10 mu m diameter; and an ausferritic matrix with sub-micron sized features, makes it ideal for prediction of mechanical properties. For that purpose, low alloyed ductile iron samples austempered between 300 and 400 degrees C for 45-180 min were tensile tested, and also multi-scale microstructural characterization were carried out using optical microscope, SEM, and EBSD technique. Moreover, a sensitivity analysis was performed to determine which microstructural parameter(s) each mechanical property is most sensitive to. The results show that tensile and yield strength are most sensitive to size and morphology of matrix phases. Moreover, the size and aspect ratio of acicular ferrite correlate well with those of high-carbon austenite; since both form during transformation of parent austenite into ausferrite during austempering treatment. Equiaxed parent austenite grains transform into ausferrite with acicular morphology during the austempering treatment; and presence of equiaxed austenite grains in the austempered samples indicates untransformed regions during austempering treatment. Ductility was found to be more sensitive to nodularity of graphite particles, and this sensitivity was attributed to the size difference between graphite particles and grain size of matrix phases.Article Investigations on the Effect of Secondary Treatments on Ti48Al2Cr2Nb Alloy Manufactured by Electron Beam Powder Bed Fusion Method(Elsevier Sci Ltd, 2025) Bilgin, Guney Mert; Ozer, Seren; Davut, Kemal; Esen, Ziya; Dericioglu, Arcan F.As-built Ti48Al2Cr2Nb alloy samples produced by electron beam powder bed fusion (PBF-EB) exhibited notable brittleness. The low ductility was attributed to coarse gamma bands aligned perpendicular to the building and tensile direction. Additionally, variations in aluminum content and hardness between the coarse colonies and fine gamma/alpha(2) lamellae contribute to this phenomenon. Electron backscattered diffraction (EBSD) studies revealed a higher amount of dislocation density and inherent strain after PBF-EB manufacturing. Hence, usage of Ti48Al2Cr2Nb alloy in the as-built condition in aviation applications with high loads and demanding environments is not found to be viable. To eliminate these negative aspects and make PBF-EB produced Ti48Al2Cr2Nb alloy available for demanding applications, two distinct post-processing heat treatments; namely, hot isostatic pressing (HIP) and annealing heat treatment (HT) were employed at 1200 degrees C. A comprehensive characterization covering microstructure analysis, EBSD, fracture surface examination, as well as room and high-temperature tensile tests allowed determination of the effect of post-processes. HIPing altered the banded structure observed in the as-built samples by increasing the amount of alpha(2) phase and grain size. On the other hand, HT made the banded structure more pronounced without significantly increasing the amount of alpha(2) phase. HT also strengthened the <001> texture, while HIPing introduced randomization of grains. On the other hand, complete recrystallization is achieved as a result of HT at 1200 degrees C for 2 h, whereas HIPing at the same temperature for 2 h induced only 80.5 % recrystallization. In both post-processes, dislocation density and inherent strain were reduced. Room temperature and high-temperature tensile tests demonstrated that both HIPing and HT eliminated the extreme brittleness of the as-built samples.Article Citation - WoS: 2Citation - Scopus: 2Microstructural Evolution and Mechanical Performance of Dual-Phase Steels Under Fiber Laser Welding: Effects of Heat Input and Weld Penetration(Springer, 2025) Tuncel, Oguz; Davut, Kemal; Aydin, HakanThis study investigates the effects of fiber laser welding (FLW) parameters on the microstructural evolution and mechanical properties of DP800, DP1000, and DP1200 dual-phase steels, focusing on the role of heat input. Welding was performed using laser powers ranging from 1500 to 3000 W and welding speeds between 20 and 100 mm/s, resulting in heat inputs from 18 to 120 J/mm. Optimal welding conditions were identified as 55 J/mm for DP800, 120 J/mm for DP1000, and 53 J/mm for DP1200, which ensured full penetration and minimized HAZ softening. Detailed microstructural analysis using SEM and EBSD revealed significant transformations in the heat-affected zone (HAZ), including martensite degradation, grain coarsening, and tempered martensite formation, particularly in DP1200 steel, where hardness reductions reached up to 29%. Tensile tests demonstrated that while DP800 and DP1000 joints primarily failed within the base material (BM) with ductile fracture characteristics, DP1200 joints fractured within the HAZ due to a combination of brittle cleavage and ductile dimples caused by martensite breakdown and carbide precipitation. The findings underscore the necessity of optimizing welding parameters to control HAZ softening and preserve mechanical performance. By systematically analyzing the interplay between heat input, microstructure, and mechanical properties across different DP steel grades, this research provides a comprehensive understanding of how FLW conditions influence joint integrity, offering valuable guidance for designing robust welding strategies in advanced engineering applications.Article Effect of Partial Austenitization Treatment on Microstructure and Mechanical Properties for Multiphase Steels(Springer, 2025) Erisir, Ersoy; Sari, Elif; Kocakusakli, Emre; Dulger, Nurten Basak; Oktay, Serkan; Tutuk, Ramazan; Davut, KemalIn this study, the microstructural evolution and mechanical properties of a 0.15 pct C-2.09 pct Mn multiphase steel was investigated. To produce a multiphase microstructure, a newly developed two-step processing of partial austenitization and quenching (PAQ) treatment was used. In the first step, the steel with initial martensitic microstructure was partially austenitized at 690 degrees C for 8 hours. After cold rolling, a rapid reheating to 840 degrees C and quenching done to simulate hot dip galvanizing conditions. To better understand the PAQ process, thermodynamic and kinetic simulations using ThermoCalc and DICTRA predicted phase transformations and elemental partitioning. Microstructural characterization via LM, SEM, and EBSD revealed an ultrafine-grained multiphase structure consisting of bainite, M/A, and intercritical ferrite. The PAQ840 sample showed an ultimate tensile strength of 740 MPa and excellent ductility with 20 pct total elongation.Article The Johnson and Cook Damage and Flow Stress Model Parameters of a Rolled Stainless Steel 304 Alloy(Elsevier, 2026) Akdogan, Ibrahim Berk; Davut, Kemal; Gueden, Mustafa; Erten, Hacer Irem; Tasdemirci, Alper; Maleki, Farshid Khosravi; Gok, Mustafa SabriPrevious studies on stainless steel 304 alloy (SS 304) have mostly focused on the stress-strain behavior as function of the volume fraction of deformation induced martensite and the applied strain and strain rate. Although equally important, the failure/fracture of this alloy has not been thoroughly investigated so far. In the present study, the Johnson and Cook (JC) damage model parameters of a rolled-SS 304 alloy, valid at a high strain rate (2900 s-1), were experimentally determined and numerically validated along with the JC flow stress parameters. The tensile failure strain of the alloy decreased as the strain rate increased from 10-3 to 10-1 s-1 and to 2900 s-1. Experimentally lower flow stresses at 2900 s-1 than at 1x10-3 s-1 were also found at the strains above 0.2, which was attributed to the adiabatic heating that declined the extend of the martensitic transformation at increasing strains. The determined damage and flow stress model parameters were further calibrated with the results of the numerical models of the quasi-static and high strain rate tension tests. Microscopic analyses and the hardness measurements on the untested and tested specimens confirmed the martensitic transformation and the highest hardness values were found in the specimens tested at 1x10-3 s-1. The martensite volume fraction as function strain rate until about necking strain (homogeneous deformation) was calculated and also microscopically determined using the electron back-scatter diffraction (EBSD) for the specimens tested at different strain rates. The results indicated the highest martensite volume fraction in the specimens tested at 10-3 s-1 (0.55-0.6) and the lowest in the specimens tested at the high strain rate (0.27-0.30). An agreement between the calculated and the EBSD determined martensite volume fractions was shown for the studied alloy.Article Citation - WoS: 1Citation - Scopus: 1Chemical Composition Optimization and Isothermal Transformation of Δ-Transformation Plasticity Steel for the Third-Generation Advanced High-Strength Steel Grade(Wiley-v C H verlag Gmbh, 2024) Okur, Onur; Davut, Kemal; Palumbo, Gianfranco; Nalcaci, Burak; Guglielmi, Pasquale; Yalcin, Mustafa Alp; Erdogan, MehmetA new low-manganese transformation-induced plasticity steel is designed with optimized nickel content to achieve superior strength and ductility while minimizing the use of expensive nickel. The steel is optimized using JMatPro software, then cast, and hot rolled. To assess the effect of intercritical annealing on austenite (martensite at room temperature) volume fraction and carbon content, hot-rolled steel samples quenched from different annealing temperatures (680-1100 degrees C) are used. Additionally, hot-rolled steel coupons are intercritically annealed at about 50% austenite formation temperature (740 degrees C) and then subjected to isothermal treatments at 300-425 degrees C for varying times (10-90 min). After optimizing these treatments to maximize retained austenite (RA), tensile specimens are heat-treated first at 740 degrees C and then isothermally at 325 degrees C. Thermodynamic calculations suggest that aluminum combined with silicon may lead to the delta ferrite formation, and even minimal nickel content can stabilize a considerable amount of austenite. In the experimental studies, it is shown that lower-temperature bainitic holding enhances austenite stability by enriching the carbon content. Optimized two-stage heat treatments yield up to 25.8% RA, with a tensile strength of 867.2 MPa and elongation of 40.6%, achieving a strength-elongation product of 35.2 GPax%, surpassing the third-generation advanced high-strength steel grades minimum requirement of 30 GPax%.Article Citation - WoS: 8Citation - Scopus: 8A Comprehensive Study of the Effect of Scanning Strategy on In939 Fabricated by Powder Bed Fusion-Laser Beam(Elsevier, 2024) Dogu, Merve Nur; Ozer, Seren; Yalcin, Mustafa Alp; Davut, Kemal; Obeidi, Muhannad Ahmed; Simsir, Caner; Brabazon, DermotThis study provides a comprehensive investigation into the effects of different scanning strategies on the material properties of IN939 fabricated using the PBF-LB process. The scanning strategies examined included alternating bi-directional scanning with rotation angles of 0 degrees, 45 degrees, 67 degrees, and 90 degrees between adjacent layers (named as shown), as well as alternating chessboard scanning with rotation angles of 67 degrees and 90 degrees (named as Q67 degrees and Q90 degrees). The results revealed that the 45 degrees and 67 degrees samples had the highest relative density, while the 0 degrees and Q67 degrees samples showed the highest average porosity. Moreover, various types of cracks, including solidification, solid-state, and oxide-induced cracks, were observed. Among the bi-directional scan samples, the 0 degrees sample displayed the most extensive cracking and the highest sigma max residual stress values in both XZ and XY planes. Conversely, the 45 degrees and 67 degrees samples exhibited fewer cracks. Notably, the lowest sigma max residual stress in the XZ planes among the bidirectional scan samples was observed in the 67 degrees sample. Additionally, microstructural analyses indicated differences in grain size and morphology, among the samples. Texture analysis indicated that the 0 degrees and 90 degrees samples exhibited strong cube textures, whereas the texture intensity weakened for the 45 degrees and 67 degrees samples. Moreover, the alternating chessboard scanning strategy led to rougher surfaces (higher Sa and Sz values) compared to the alternating bi-directional scanning strategy, regardless of the rotation angles. Furthermore, the microhardness values among the samples showed minimal variance, ranging between 321 + 14 HV and 356+ 7 HV.Article Citation - WoS: 1Citation - Scopus: 1Effect of Mn Concentration on Mechanical Properties of A356 Aluminum Alloy Wheels Produced by Low-Pressure Die Casting(Springer int Publ Ag, 2024) Kaya, A. Yigit; Davut, Kemal; Gokelma, MertolSecondary aluminum alloys in automotive industry have been rising in last decades; however, the iron content is still a concern whether recycled or high iron containing aluminum alloys can fulfill the mechanical requirements. As the proportion of recycled scrap increases in aluminum alloy components, the mixing and accumulation of impurities become significant issues. In this study, manganese was used to counteract the detrimental effects of iron. Accordingly, A356 alloy automobile wheels containing 0.002 wt%, 0.040 wt%, 0.069 wt%, and 0.14 wt% Mn were cast using the low-pressure die casting method, followed by T6 heat treatment. Optical microscope (OM) examinations were performed to observe intermetallics. Additionally, the mechanical properties of the produced wheels were evaluated through hardness measurements, tensile, and Charpy impact tests. After the Charpy impact test, fractured surfaces were examined using scanning electron microscopy (SEM). Micrographs from SEM and OM were quantified using digital image processing. To interpret this extensive dataset, a statistical model was developed using microstructural data as input through multiple linear regression analysis and analysis of variance. The results were discussed together with the sensitivity analysis. A weak negative linear correlation between Mn concentration and mechanical properties was found, indicating that Mn addition is not the primary factor for the observed decrease in mechanical properties. Elongation and yield strength were significantly influenced by both aspect ratio and particles/mm2, with greater sensitivity to particles/mm2. Additionally, impact energy was strongly affected by aspect ratio of particles (intermetallics and eutectic Si) and their concentration per unit area.Article Citation - WoS: 6Citation - Scopus: 6Comparison of Linear and Nonlinear Twist Extrusion Processes With Crystal Plasticity Finite Element Analysis(Mdpi, 2024) Simsek, Ulke; Davut, Kemal; Miyamoto, Hiroyuki; Yalcinkaya, TuncayThe mechanical characteristics of polycrystalline metallic materials are influenced significantly by various microstructural parameters, one of which is the grain size. Specifically, the strength and the toughness of polycrystalline metals exhibit enhancement as the grain size is reduced. Applying severe plastic deformations (SPDs) has a noticeable result in obtaining metallic materials with ultrafine-grained (UFG) microstructure. SPD, executed through conventional shaping methods like extrusion, plays a pivotal role in the evolution of the texture, which is closely related to the plastic behavior and ductility. A number of SPD processes have been developed to generate ultrafine-grained materials, each having a different shear deformation mechanism. Among these methods, linear twist extrusion (LTE) presents a non-uniform and non-monotonic form of severe plastic deformation, leading to significant shifts in the microstructure. Prior research demonstrates the capability of the LTE process to yield consistent, weak textures in pre-textured copper. However, limitations in production efficiency and the uneven distribution of grain refinement have curbed the widespread use of LTE in industrial settings. This has facilitated the development of an improved novel method, that surpasses the traditional approach, known as the nonlinear twist extrusion procedure (NLTE). The NLTE method innovatively adjusts the channel design of the mold within the twist section to mitigate strain reversal and the rotational movement of the workpiece, both of which have been identified as shortcomings of twist extrusion. Accurate anticipation of texture changes in SPD processes is essential for mold design and process parameter optimization. The performance of the proposed extrusion technique should still be studied. In this context, here, a single crystal (SC) of copper in billet form, passing through both LTE and NLTE, is analyzed, employing a rate-dependent crystal plasticity finite element (CPFE) framework. CPFE simulations were performed for both LTE and NLTE of SC copper specimens having <100> or <111> directions parallel to the extrusion direction initially. The texture evolution as well as the cross-sectional distribution of the stress and strain is studied in detail, and the performance of both processes is compared.Article Citation - WoS: 11Citation - Scopus: 11A Comprehensive Characterization of the Effect of Spatter Powder on In939 Parts Fabricated by Laser Powder Bed Fusion(ELSEVIER SCI LTD, 2023) Dogu, Merve Nur; Mussatto, Andre; Yalçın, Mustafa Alp; Özer, Seren; Davut, Kemal; Obeidi, Muhannad Ahmed; Kumar, AjayThis study is focused on a comprehensive characterization of virgin and spatter IN939 powders and the effects of a certain amount of spatter powder on the part quality of IN939 fabricated by the L-PBF process. A brown tint coloration formed Al2O3 oxide, pores, a 124.4% increase in the average particle size, a 10.2% decrease in the powder circularity, and a 7.5% decrease in the powder aspect ratio were observed in the spatter powder. Additionally, higher average grain size and lower nanohardness were obtained for the spatter powder. In order to understand the effect of a certain amount of spatter powder on the part quality, 10 wt% spatter powder was mixed with the virgin powder. This addition was found to decrease the flowability of the powder. Moreover, this addition decreased relative density by around 0.3% and increased surface roughness by around 80.8% in the fabricated samples (termed as V and SV). On the other hand, there was no considerable microstructural, texture, microhardness, and nanohardness difference between V and SV samples, although the spatter powder addition caused a 30.2% increase in the average grain size of SV. The overall texture for both V and SV samples exhibit (00 1)//BD.