Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection

Permanent URI for this collectionhttps://hdl.handle.net/11147/7148

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  • Article
    Citation - WoS: 3
    Citation - Scopus: 4
    Phase Formation and Microstructure of Nd +3 Doped Pb(mg 1/3nb 2/3)o 3 Prepared by Sol-Gel Method
    (Springer Verlag, 2008) Şakar-Deliormanlı, Aylin; Polat, Mehmet; Çelik, Erdal; Şakar Deliormanlı, Aylin Müyesser; Polat, Mehmet; 03.02. Department of Chemical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of Technology
    The aim of this study was to investigate the effects of the rare earth element neodymium on the phase formation and microstructural development of relaxor ferroelectric lead magnesium niobate, Pb(Mg 1/3 Nb 2/3)O 3 (PMN) system. Perovskite phase PMN powders were prepared using the sol - gel method and the effect of neodymium doping was investigated at different doping levels ranging from 0.1 mol% to 30 mol%. The precursors employed in the sol - gel process were lead (II) acetate, magnesium ethoxide, and niobium (V) ethoxide. All the experiments were performed at room temperature while the calcination temperatures ranged between 800 °C and 1,100 °C. Results showed that it was possible to obtain the pure perovskite phase at 950 °C using the sol - gel method. Nd +3 addition influenced the phase formation and microstructure of the multicomponent system. Pyrochlore was detected along with the perovskite phase above 10 mol% Nd. Results also demonstrated that grain size of the synthesized powders depended on the Nd +3 concentration.
  • Article
    Citation - WoS: 67
    Citation - Scopus: 82
    Microhardness and Fracture Toughness of Dental Materials by Indentation Method
    (John Wiley and Sons Inc., 2005) Şakar-Deliormanlı, Aylin; Şakar Deliormanlı, Aylin Müyesser; Güden, Mustafa; Güden, Mustafa; 03.02. Department of Chemical Engineering; 03.10. Department of Mechanical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of Technology
    The main objective of this study was to measure the fracture toughness of the human teeth enamel using the microindentation technique and to compare the results calculated from the equations developed for Palmqvist and radial-median cracks. Vickers microhardness measurements of dental ceramic (alumina) and human teeth were performed using indentation fracture method. The fracture toughness of enamel was calculated using different equations reported in the literature. Vickers microhardness of the sintered alumina specimen (98.8% theoretical density) was measured to be 14.92 GPa under 9.8N indentation load. Three equations based on the radial-median cracks were found to be applicable for the fracture toughness determination of the enamel. Results show that indentation fracture method is adequate to measure microhardness and fracture toughness of dental materials. However the calculation of fracture toughness depended on the nature of the cracks and also on the location of the indentation. Therefore, it is necessary to identify the crack profile and to select the appropriate equation for accurate fracture toughness values.