Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
Permanent URI for this collectionhttps://hdl.handle.net/11147/7148
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Article Citation - WoS: 1Citation - Scopus: 1The Separation Behavior of Tib<sub>2</Sub> During Cl<sub>2</Sub>-free Degassing Treatment of 5083 Aluminum Melt(Mdpi, 2024) Li, Cong; Gokelma, Mertol; Stets, Wolfram; Friedrich, BerndUtilizing titanium diboride (TiB2) inoculation for grain-refining purposes is a widely established practice in aluminum casthouses and foundries. Since this inoculation is usually implemented jointly with or between routine melt treatment steps ahead of casting, it is important to know whether and how other melt treatment processes affect the fade of TiB2 particles. For the present study, we investigated the influence of degassing process on the separation behavior of TiB2 particles in aluminum melt. Multiple sampling methods were employed and the samples were analyzed via spectrometer analysis. The removal efficiency of TiB2 during the gas-purging process of 5083 aluminum melt was confirmed to be significant over 10 min of treatment time. The rate at which the TiB2 content decays was found to increase with the impeller rotary speed from 400 rounds per minute (rpm) to 700 rpm. The separation rate of TiB2 particles was obtained to be 0.05-0.08 min(-1) by fitting the experimental data. Particle mapping results suggest that the TiB2 particles were separated to a dross layer. The obtained experimental results were used to quantitatively evaluate the conventional deterministic flotation model. The deviation between the conventional model and the experimental data was explained through the entrainment-entrapment (EE) model. Suggestions were made for future analytical and experimental works which may validate the EE model.Conference Object Citation - WoS: 1Citation - Scopus: 1Assessment of Separation and Agglomerationt Tendency of Non-Metallic Inclusions in an Electromagnetically Stirred Aluminum Melt(Springer international Publishing Ag, 2023) Li, Cong; Dang, Thien; Gokelma, Mertol; Zimmermann, Sebastian; Mitterecker, Jonas; Friedrich, BerndPresence of non-metallic inclusions (NMIs) reduces surface quality and mechanical properties of aluminum products. The development of good NMIs removal practices relies on the understanding of inclusion behaviors with respect to separation and agglomeration particularly in the turbulent flow. In the scenario of electromagnetically induced recirculated turbulent flow, the concerned behaviors of inclusions with different sizes have rarely been investigated experimentally. In the presented study funded by AMAP Open Innovation Research Cluster, reference materials were prepared with uniformly distributed NMIs (SiC and MgAl2O4) via an ultrasoundinvolved casting route. Reference materials were charged into an aluminum melt where turbulent flow was promoted via electromagnetic force. Microscopical analysis shows non-significant agglomeration tendency of SiC, MgAl2O4, and TiB2 inclusion. Time-weight filtration curve, PoDFA, and Spark Spectrometer results suggest a strong dependence of separation rate on particle size. Analytical models were established to estimate the collision rate of particles and to evaluate separation probability of different sized particles.Article Citation - WoS: 10Citation - Scopus: 7Assessment of Melt Cleanliness of Secondary 5000 Aluminum Alloy Via Non-Metallic Inclusions Characterization(Springer, 2023) Li, Cong; Dang, Thien; Huang, Jinxian; Huang, Chunfa; Li, Jianguo; Friedrich, Bernd; Gökelma, MertolThe extensive energy consumption of primary aluminum production stimulates increasing need of producing primary-quality alloys with secondary sources, during which process amount of non-metallic inclusions (NMIs) in the alloy must be strictly controlled. In the present study funded by AMAP Open Innovation Research Cluster, NMIs generated during remelting a 5000 Al-Mg alloy was investigated to offer benchmarking characters of NMIs with respect to type, morphology, size, composition, and concentration. Under different remelting conditions NMIs formed in the melt ahead of solidification were concentrated using Porous Disc Filtration Apparatus (PoDFA) and characterized microstructurally and quantitatively. Investigated conditions included heating cycle, organic contaminations, and refractory materials. Results suggested oxide films and cuboid particles as typical oxides with, respectively, different compositions. The amount of formed oxides declined with the increase of heating rate. With respect to aluminum carbide (Al4C3), organic contaminations were confirmed to lead to an increased amount of its formation. The carbon-containing refractory material contributed more significantly than organic contaminations on the formation of Al4C3 at melt temperatures over 760 & DEG;C. Formulas were derived based on trial results to enable translation of NMIs PoDFA value [mm(2)/kg] into their mass fraction [ppm] in the melt.