Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection
Permanent URI for this collectionhttps://hdl.handle.net/11147/7148
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Article Microstructure-Based Prediction of Mechanical Properties of Austempered Ductile Iron Using Multiple Linear Regression Analysis(Springer int Publ Ag, 2025) Yalcin, M. Alp; Davut, KemalMultiple linear regression analysis (MLRA) was used to predict the mechanical properties of austempered ductile iron (ADI) including yield and tensile strength, uniform elongation, hardening exponent, as well as fracture energy by building a model that uses characteristic features of microstructural constituents as input parameters. The complex multi-scale microstructure of ADI, which is composed of spherical graphite particles over 10 mu m diameter; and an ausferritic matrix with sub-micron sized features, makes it ideal for prediction of mechanical properties. For that purpose, low alloyed ductile iron samples austempered between 300 and 400 degrees C for 45-180 min were tensile tested, and also multi-scale microstructural characterization were carried out using optical microscope, SEM, and EBSD technique. Moreover, a sensitivity analysis was performed to determine which microstructural parameter(s) each mechanical property is most sensitive to. The results show that tensile and yield strength are most sensitive to size and morphology of matrix phases. Moreover, the size and aspect ratio of acicular ferrite correlate well with those of high-carbon austenite; since both form during transformation of parent austenite into ausferrite during austempering treatment. Equiaxed parent austenite grains transform into ausferrite with acicular morphology during the austempering treatment; and presence of equiaxed austenite grains in the austempered samples indicates untransformed regions during austempering treatment. Ductility was found to be more sensitive to nodularity of graphite particles, and this sensitivity was attributed to the size difference between graphite particles and grain size of matrix phases.Article Citation - WoS: 2Citation - Scopus: 2Microstructural Evolution and Mechanical Performance of Dual-Phase Steels Under Fiber Laser Welding: Effects of Heat Input and Weld Penetration(Springer, 2025) Tuncel, Oguz; Davut, Kemal; Aydin, HakanThis study investigates the effects of fiber laser welding (FLW) parameters on the microstructural evolution and mechanical properties of DP800, DP1000, and DP1200 dual-phase steels, focusing on the role of heat input. Welding was performed using laser powers ranging from 1500 to 3000 W and welding speeds between 20 and 100 mm/s, resulting in heat inputs from 18 to 120 J/mm. Optimal welding conditions were identified as 55 J/mm for DP800, 120 J/mm for DP1000, and 53 J/mm for DP1200, which ensured full penetration and minimized HAZ softening. Detailed microstructural analysis using SEM and EBSD revealed significant transformations in the heat-affected zone (HAZ), including martensite degradation, grain coarsening, and tempered martensite formation, particularly in DP1200 steel, where hardness reductions reached up to 29%. Tensile tests demonstrated that while DP800 and DP1000 joints primarily failed within the base material (BM) with ductile fracture characteristics, DP1200 joints fractured within the HAZ due to a combination of brittle cleavage and ductile dimples caused by martensite breakdown and carbide precipitation. The findings underscore the necessity of optimizing welding parameters to control HAZ softening and preserve mechanical performance. By systematically analyzing the interplay between heat input, microstructure, and mechanical properties across different DP steel grades, this research provides a comprehensive understanding of how FLW conditions influence joint integrity, offering valuable guidance for designing robust welding strategies in advanced engineering applications.Article Effect of Partial Austenitization Treatment on Microstructure and Mechanical Properties for Multiphase Steels(Springer, 2025) Erisir, Ersoy; Sari, Elif; Kocakusakli, Emre; Dulger, Nurten Basak; Oktay, Serkan; Tutuk, Ramazan; Davut, KemalIn this study, the microstructural evolution and mechanical properties of a 0.15 pct C-2.09 pct Mn multiphase steel was investigated. To produce a multiphase microstructure, a newly developed two-step processing of partial austenitization and quenching (PAQ) treatment was used. In the first step, the steel with initial martensitic microstructure was partially austenitized at 690 degrees C for 8 hours. After cold rolling, a rapid reheating to 840 degrees C and quenching done to simulate hot dip galvanizing conditions. To better understand the PAQ process, thermodynamic and kinetic simulations using ThermoCalc and DICTRA predicted phase transformations and elemental partitioning. Microstructural characterization via LM, SEM, and EBSD revealed an ultrafine-grained multiphase structure consisting of bainite, M/A, and intercritical ferrite. The PAQ840 sample showed an ultimate tensile strength of 740 MPa and excellent ductility with 20 pct total elongation.Article The Johnson and Cook Damage and Flow Stress Model Parameters of a Rolled Stainless Steel 304 Alloy(Elsevier, 2026) Akdogan, Ibrahim Berk; Davut, Kemal; Gueden, Mustafa; Erten, Hacer Irem; Tasdemirci, Alper; Maleki, Farshid Khosravi; Gok, Mustafa SabriPrevious studies on stainless steel 304 alloy (SS 304) have mostly focused on the stress-strain behavior as function of the volume fraction of deformation induced martensite and the applied strain and strain rate. Although equally important, the failure/fracture of this alloy has not been thoroughly investigated so far. In the present study, the Johnson and Cook (JC) damage model parameters of a rolled-SS 304 alloy, valid at a high strain rate (2900 s-1), were experimentally determined and numerically validated along with the JC flow stress parameters. The tensile failure strain of the alloy decreased as the strain rate increased from 10-3 to 10-1 s-1 and to 2900 s-1. Experimentally lower flow stresses at 2900 s-1 than at 1x10-3 s-1 were also found at the strains above 0.2, which was attributed to the adiabatic heating that declined the extend of the martensitic transformation at increasing strains. The determined damage and flow stress model parameters were further calibrated with the results of the numerical models of the quasi-static and high strain rate tension tests. Microscopic analyses and the hardness measurements on the untested and tested specimens confirmed the martensitic transformation and the highest hardness values were found in the specimens tested at 1x10-3 s-1. The martensite volume fraction as function strain rate until about necking strain (homogeneous deformation) was calculated and also microscopically determined using the electron back-scatter diffraction (EBSD) for the specimens tested at different strain rates. The results indicated the highest martensite volume fraction in the specimens tested at 10-3 s-1 (0.55-0.6) and the lowest in the specimens tested at the high strain rate (0.27-0.30). An agreement between the calculated and the EBSD determined martensite volume fractions was shown for the studied alloy.Article Citation - WoS: 3Citation - Scopus: 3Influence of Oscillating Fiber Laser Welding Process Parameters on the Fatigue Response and Mechanical Performance of Butt-Jointed Twip980 Steels(Walter de Gruyter Gmbh, 2025) Cavusoglu, Oktay; Aydin, Hakan; Eroglu, Mehmet; Davut, KemalIn this study, the effect of laser power, welding speed, linear heat inputs on the mechanical performance of TWIP980 steels joined by oscillating fiber laser welding in butt welding configuration was investigated. Oscillating fiber laser welding were changed: laser power from 1.2 to 1.6 kW, welding speed from 20 to 30 mm s-1, linear heat input from 40 to 80 J mm-1. The tensile, hardness and fatigue tests were carried out to determine mechanical performance. A significant improvement in weld penetration, fatigue performance and mechanical properties was detected at linear heat inputs above 53.33 J mm-1. The best mechanical properties were obtained at 1.6 kW laser power and 25 mm s-1 welding speed. The study reveals that linear heat inputs, laser power, and welding speed have significant effects on mechanical performance and weld geometry. Furthermore, the results demonstrate that oscillating fiber laser welding enables good weldability even at low laser power.Article Citation - WoS: 1Citation - Scopus: 1Effect of Mn Concentration on Mechanical Properties of A356 Aluminum Alloy Wheels Produced by Low-Pressure Die Casting(Springer int Publ Ag, 2024) Kaya, A. Yigit; Davut, Kemal; Gokelma, MertolSecondary aluminum alloys in automotive industry have been rising in last decades; however, the iron content is still a concern whether recycled or high iron containing aluminum alloys can fulfill the mechanical requirements. As the proportion of recycled scrap increases in aluminum alloy components, the mixing and accumulation of impurities become significant issues. In this study, manganese was used to counteract the detrimental effects of iron. Accordingly, A356 alloy automobile wheels containing 0.002 wt%, 0.040 wt%, 0.069 wt%, and 0.14 wt% Mn were cast using the low-pressure die casting method, followed by T6 heat treatment. Optical microscope (OM) examinations were performed to observe intermetallics. Additionally, the mechanical properties of the produced wheels were evaluated through hardness measurements, tensile, and Charpy impact tests. After the Charpy impact test, fractured surfaces were examined using scanning electron microscopy (SEM). Micrographs from SEM and OM were quantified using digital image processing. To interpret this extensive dataset, a statistical model was developed using microstructural data as input through multiple linear regression analysis and analysis of variance. The results were discussed together with the sensitivity analysis. A weak negative linear correlation between Mn concentration and mechanical properties was found, indicating that Mn addition is not the primary factor for the observed decrease in mechanical properties. Elongation and yield strength were significantly influenced by both aspect ratio and particles/mm2, with greater sensitivity to particles/mm2. Additionally, impact energy was strongly affected by aspect ratio of particles (intermetallics and eutectic Si) and their concentration per unit area.Article Citation - WoS: 6Citation - Scopus: 6Comparison of Linear and Nonlinear Twist Extrusion Processes With Crystal Plasticity Finite Element Analysis(Mdpi, 2024) Simsek, Ulke; Davut, Kemal; Miyamoto, Hiroyuki; Yalcinkaya, TuncayThe mechanical characteristics of polycrystalline metallic materials are influenced significantly by various microstructural parameters, one of which is the grain size. Specifically, the strength and the toughness of polycrystalline metals exhibit enhancement as the grain size is reduced. Applying severe plastic deformations (SPDs) has a noticeable result in obtaining metallic materials with ultrafine-grained (UFG) microstructure. SPD, executed through conventional shaping methods like extrusion, plays a pivotal role in the evolution of the texture, which is closely related to the plastic behavior and ductility. A number of SPD processes have been developed to generate ultrafine-grained materials, each having a different shear deformation mechanism. Among these methods, linear twist extrusion (LTE) presents a non-uniform and non-monotonic form of severe plastic deformation, leading to significant shifts in the microstructure. Prior research demonstrates the capability of the LTE process to yield consistent, weak textures in pre-textured copper. However, limitations in production efficiency and the uneven distribution of grain refinement have curbed the widespread use of LTE in industrial settings. This has facilitated the development of an improved novel method, that surpasses the traditional approach, known as the nonlinear twist extrusion procedure (NLTE). The NLTE method innovatively adjusts the channel design of the mold within the twist section to mitigate strain reversal and the rotational movement of the workpiece, both of which have been identified as shortcomings of twist extrusion. Accurate anticipation of texture changes in SPD processes is essential for mold design and process parameter optimization. The performance of the proposed extrusion technique should still be studied. In this context, here, a single crystal (SC) of copper in billet form, passing through both LTE and NLTE, is analyzed, employing a rate-dependent crystal plasticity finite element (CPFE) framework. CPFE simulations were performed for both LTE and NLTE of SC copper specimens having <100> or <111> directions parallel to the extrusion direction initially. The texture evolution as well as the cross-sectional distribution of the stress and strain is studied in detail, and the performance of both processes is compared.Article Citation - WoS: 5Citation - Scopus: 4Influence of Partitioning Treatment on Microstructure and Mechanical Properties of an Alloyed Ductile Iron Austempered at Different Temperatures(Walter de Gruyter GmbH, 2023) Neite, Maximilian; Münstermann, Sebastian; Nalçacı, Burak; Davut, Kemal; Erdoğan, MehmetThe present study was conducted to uncover effects of partitioning treatment on Cu-Ni-Mo alloyed ductile iron (DI) austempered at different temperatures. For this purpose, the DI samples, produced via sand casting, were austenitized at 900 °C for 60 min, followed by austempering at the temperatures of 275-325-375 °C for 120 min and afterwards a partitioning treatment was applied at 200 °C for 15 min. In the characterization studies, dilatometer, image analysis, JMat-Pro, mechanical tests, XRD, optical microscope, and scanning electron microscope (SEM) equipped with EBSD detector were utilized. Characterization studies showed that the effects of partitioning treatment were directly correlated with austempering temperature and high carbon austenite volume fraction changed in the range of 19.48-35.45%. That redistribution of carbon (C) between bainitic ferrite and high carbon austenite occurred, in turn, the carbon content of high carbon austenite increased with the partitioning treatment irrespective of austempering temperature were uncovered. Furthermore, the partitioning treatment considerably changed the grain morphologies of both high carbon austenite and banitic ferrite. As a consequence of these microstructural differences, the highest tensile strength of 1489.2 MPa was established in the sample austempered at 275 °C and partitioned at 200 °C, whereas the highest ductility of 5.61% acquired at the austempering temperature of 375 °C. © 2023 Walter de Gruyter GmbH, Berlin/Boston.Article Citation - WoS: 3Citation - Scopus: 3Nondestructive Microstructural Characterization of Austempered Ductile Iron(Walter de Gruyter GmbH, 2023) Tüzün, Mert Yağız; Yalçın, Mustafa Alp; Davut, Kemal; Kılıçlı, VolkanAustempered ductile iron (ADI) has been preferred in a wide range of applications due its unique combination of high strength, good ductility, wear resistance and fracture toughness together with lower cost and lower density compared to steels. Magnetic Barkhausen noise (MBN) measurement offers a better alternative to traditional characterization techniques by being fast and non-destructive. A simple linear regression using only one single independent variable cannot correlate the MBN with the microstructure of ADI, since its microstructure is multi component. Multiple linear regression analysis (MLRA) was used to build a model that uses the characteristic features of microstructural constituents as input parameters to predict the MBN. For that purpose, Cu-Ni-Mo alloyed ductile iron samples austempered between 325 and 400 degrees C and for 45-180 min duration were used. The results show that MBN is most sensitive to the size and shape of acicular ferrite and retained austenite. Moreover, MBN is almost insensitive to the size, morphology and volume fraction of graphite particles. This indicates that retained austenite pins the domain walls more effectively than the graphite particles. Considering the results MLRA, MBN technique can be used to characterize the ausferritic microstructure of ADI.Article Citation - WoS: 6Citation - Scopus: 6Texture Evolution of Friction Stir-Processed Dual-Phase Steel(Springer, 2022) Aktarer, Semih Mahmut; Küçükömeroğlu, Tevfik; Davut, KemalEvolution of crystallographic texture and local strains in different zones of a dual-phase steel subjected to severe plastic deformation by friction stir process was examined by electron backscatter diffraction technique. Misorientations, which were expressed by the values of grain orientation spread and kernel average misorientation (KAM), increased from the thermomechanical affected zone (TMAZ) to pin-affected stir zone (PE-SZ). KAM maps showed that the highest local strain appeared in the PE-SZ. Misorientation distributions were found to be consistent with microhardness distributions in the processed region. The crystallographic texture of base metal, heat-affected zone, and TMAZ was similar. Recrystallization and deformation texture components were observed at stir zones, and recrystallization texture components decreased drastically at PE-SZ. Rotated cube, goss and rotated goss texture components were detected at PE-SZ. Rotated cube texture component indicates partial recrystallization after plastic deformation. Shear texture components were determined using shear direction (SD) as reference. Different shear texture components (111), (112), and (101)