Scopus İndeksli Yayınlar Koleksiyonu / Scopus Indexed Publications Collection

Permanent URI for this collectionhttps://hdl.handle.net/11147/7148

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Now showing 1 - 5 of 5
  • Article
    Citation - WoS: 5
    Citation - Scopus: 5
    Mechanical Properties of Palygorskite Clay Stabilized With Polyelectrolytes
    (Elsevier, 2023) Huang, Jianxin; Makhatova, Ardak; Kogbara, Reginald; Masad, Eyad; Sukhishvili, Svetlana; Little, Dallas
    Two polyelectrolytes of opposite charges, sodium polystyrene sulfonate (PSS) and polydiallyldimethylammonium chloride (PDADMAC), were investigated to stabilize palygorskite clay at varying dosages of 0.2, 0.8, 1.6, and 3.2 % by the dry weight of the soil. Both PSS and PDADMAC improved the unconfined compressive strength of the palygorskite clay. PSS was effective at all the polymer contents studied after 7 days of dry curing and the strength increased with the dosages of PSS added, ranging from 2 MPa (0.2 % PSS) to 3.1 MPa (3.2 % PSS), compared with 1.5 MPa of the untreated soil. PDADMAC, on the other hand, showed comparable strength improvements as PSS did at the high polymer contents of 1.6 and 3.2 % but did not work at 0.2 and 0.8 % dosages. Under wet curing at 100 % relative humidity, PSS improved the strength of the clay by 40 % (620 kPa at 0.2 % PSS) to 77 % (764 kPa at 1.6 % PSS) compared to the untreated clay (440 kPa). PDADMAC exhibited less improvement than PSS under wet conditions but still worked at dosages of 0.8 and 1.6 %. Besides strength, the resilient modulus and fracture toughness of the treated specimens increased by approximately 10 % and 66 %, respectively, when treated with 1.6 % PSS, which was the optimum content based on the strength results. PDADMAC-treated palygorskite, however, exhibited cracking during curing for both tests, showing potential drying crack issues. The adsorption of PSS and PDADMAC on palygorskite clay were also measured using ultraviolet–visible spectroscopy, and binding between these polymers and palygorskite has been confirmed. The measured adsorption capacities of PSS and PDADMAC were comparable (2.9 and 2.7 mg/g, respectively), while the PSS was somewhat more efficient in improving soil mechanical properties. © 2023 Elsevier Ltd
  • Article
    Citation - WoS: 97
    Citation - Scopus: 110
    Effect of Polyamide-6,6 (pa 66) Nonwoven Veils on the Mechanical Performance of Carbon Fiber/Epoxy Composites
    (Elsevier Ltd., 2018) Beylergil, Bertan; Tanoğlu, Metin; Aktaş, Engin
    In this study, carbon fiber/epoxy (CF/EP) composites were interleaved with polyamide-6,6 (PA 66) nonwoven veils at two different areal weight densities (17 and 50 gsm) to improve their delamination resistance against Mode-I loading. Mode-I fracture toughness (DCB), tensile, open hole tensile (OHT), flexural, compression, short beam shear (ILSS) and Charpy-impact tests were performed on the reference and PA 66 interleaved composite specimens. The DCB test results showed that the initiation and propagation Mode-I fracture toughness values of the composites were significantly improved by 84 and 171% using PA 66-17 gsm veils respectively, as compared to reference laminates. The use of denser PA 66-50 gsm veils in the interlaminar region led to higher improvement in fracture toughness values (349% for initiation and 718% for propagation) due to the higher amount of veil fibers involved in fiber bridging toughening mechanism. The incorporation of PA 66-50 gsm nonwoven veils also increased the ILSS and Charpy impact strength of the composites by 25 and 15%, respectively. On the other hand, the PA 66 veils reduced in-plane mechanical properties of CF/EP composites due to lower carbon fiber volume fraction and increased thickness.
  • Article
    Citation - WoS: 73
    Citation - Scopus: 92
    Tensile Mechanical Behavior and Fracture Toughness of Mwcnt and Dwcnt Modified Vinyl-ester/Polyester Hybrid Nanocomposites Produced by 3-Roll Milling
    (Elsevier Ltd., 2009) Seyhan, Abdullah Tuğrul; Tanoğlu, Metin; Schulte, Karl
    This study aims to investigate the tensile mechanical behavior and fracture toughness of vinyl-ester/polyester hybrid nanocomposites containing various types of nanofillers, including multi- and double-walled carbon nanotubes with and without amine functional groups (MWCNTs, DWCNTs, MWCNT-NH2 and DWCNT-NH2). To prepare the resin suspensions, very low contents (0.05, 0.1 and 0.3 wt.%) of carbon nanotubes (CNTs) were dispersed within a specially synthesized styrene-free polyester resin, conducting 3-roll milling technique. The collected resin stuff was subsequently blended with vinyl-ester via mechanical stirring to achieve final suspensions prior to polymerization. Nanocomposites containing MWCNTs and MWCNT-NH2 were found to exhibit higher tensile strength and modulus as well as larger fracture toughness and fracture energy compared to neat hybrid polymer. However, incorporation of similar contents of DWCNTs and DWCNT-NH2 into the hybrid resin did not reflect the same improvement in the corresponding mechanical properties. Furthermore, experimentally measured elastic moduli of the nanocomposites containing DWCNTs, DWCNT-NH2, MWCNTs and MWCNT-NH2 were fitted to Halphin-Tsai model. Regardless of amine functional groups or content of carbon nanotubes, MWCNT modified nanocomposites exhibited better agreement between the predicted and the measured elastic moduli values compared to nanocomposites with DWCNTs. Furthermore, Transmission Electron Microscopy (TEM) and Scanning Electron Microscopy (SEM) were used to reveal dispersion state of the carbon nanotubes within the hybrid polymer and to examine the CNT induced failure modes that occurred under mechanical loading, respectively. Based on the experimental findings obtained, it was emphasized that the types of CNTs and presence of amine functional groups on the surface of CNTs affects substantially the chemical interactions at the interface, thus tuning the ultimate mechanical performance of the resulting nanocomposites.
  • Article
    Citation - WoS: 24
    Citation - Scopus: 26
    Cure Kinetics of Vapor Grown Carbon Nanofiber (vgcnf) Modified Epoxy Resin Suspensions and Fracture Toughness of Their Resulting Nanocomposites
    (Elsevier Ltd., 2009) Seyhan, Abdullah Tuğrul; Sun, Z.; Deitzel, J.; Tanoğlu, Metin; Heider, D.
    In this study, the cure kinetics of Cycom 977-20, an aerospace grade toughened epoxy resin, and its suspensions containing various amounts (1, 3 and 5 wt.%) of vapor grown carbon nanofibers (VGCNFs) with and without chemical treatment were monitored via dynamic and isothermal dynamic scanning calorimetry (DSC) measurements. For this purpose, VGCNFs were first oxidized in nitric acid and then functionalized with 3-glycidoxypropyltrimethoxy silane (GPTMS) coupling agent. Fourier transform infrared (FTIR) spectroscopy was subsequently used to verify the chemical functional groups grafted onto the surfaces of VGCNFs. Sonication technique was conducted to facilitate proper dispersion of as-received, acid treated and silanized VGCNFs within epoxy resin. Dynamic DSC measurements showed that silanized VGCNF modified resin suspensions exhibited higher heat of cure compared to those with as-received VGCNFs. Experimentally obtained isothermal DSC data was then correlated with Kamal phenomenological model. Based on the model predictions, it was found that silanized VGCNFs maximized the cure reaction rates at the very initial stage of the reaction. Accordingly, an optimized curing cycle was applied to harden resin suspensions. Fracture testing was then carried out on the cured samples in order to relate the curing behavior of VGCNF modified resin suspensions to mechanical response of their resulting nanocomposites. With addition of 1 wt.% of silanized VGCNFs, the fracture toughness value of neat epoxy was found to be improved by 12%. SEM was further employed to examine the fracture surfaces of the samples.
  • Article
    Citation - WoS: 182
    Citation - Scopus: 214
    Mode I and Mode Ii Fracture Toughness of E-Glass Non-Crimp Fabric/Carbon Nanotube (cnt) Modified Polymer Based Composites
    (Elsevier Ltd., 2008) Seyhan, Abdullah Tuğrul; Tanoğlu, Metin; Schulte, Karl
    In this study, mode I and mode II interlaminar fracture toughness, and interlaminar shear strength of E-glass non-crimp fabric/carbon nanotube modified polymer matrix composites were investigated. The matrix resin containing 0.1 wt.% of amino functionalized multi walled carbon nanotubes were prepared, utilizing the 3-roll milling technique. Composite laminates were manufactured via vacuum assisted resin transfer molding process. Carbon nanotube modified laminates were found to exhibit 8% and 11% higher mode II interlaminar fracture toughness and interlaminar shear strength values, respectively, as compared to the base laminates. However, no significant improvement was observed for mode I interlaminar fracture toughness values. Furthermore, Optical microscopy and scanning electron microscopy were utilized to monitor the distribution of carbon nanotubes within the composite microstructure and to examine the fracture surfaces of the failed specimens, respectively. © 2008 Elsevier Ltd. All rights reserved.