WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
Permanent URI for this collectionhttps://hdl.handle.net/11147/7150
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Article Citation - WoS: 2The Effect of the Temperature of Heat Treatment Process and the Concentration and Duration of Acid Leaching on the Size and Crystallinity of Nano-Silica Powders Formed by the Dissociation of Natural Diatom Frustule(American Scientific Publishers, 2022) Güden, Mustafa; Güden, Mustafa; 03.10. Department of Mechanical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of TechnologyThe present study focused on the processing of nano-silica powders in varying sizes and crystallinities through IP: 846247.10 On: Wed, 14 Dec 2022 07:29:25 heat treatment (900-1200 degrees C), hydrofluoric acid leaching (1-7 N), and ball milling (1 h, 500 rpm) of natural Copyright American Scentfic P blishers diatom frustules. The starting natural frustules were determined to be composed of amorphous silica (88%) Delivered by Ingenta and quartz. The partially ordered crystalline low-quartz and or precursor to low-cristobalite started to form at-900 degrees C. As the heat treatment temperature increased, the crystallinity of the frustules increased from 9.3% at 25 degrees C to 46% at 1200 degrees C. Applying a ball milling reduced the mean particle sizes of the as-received and heat-treated frustules from 15.6-13.7 mu m to 7.2-6.7 mu m, respectively. Acid leaching of the as-received and heat-treated frustules resulted in a further increase in the crystallinity. Furthermore, a ball milling applied after an acid leaching was very effective in reducing the particle size of the as-received and heat-treated frustules. The mean particle size of the acid-leached frustules decreased to 774-547 nm with a crystallinity varying between 12 and 48% after ball milling. A partially dissolved amorphous phase was observed in between crystalline silica grains after acid leaching, which resulted in a rapid fracture/separation of the frustules in ball milling.Article Citation - WoS: 12Citation - Scopus: 15Effect of Heat Treatment on the Blast Loading Response of Combined Geometry Shell Core Sandwich Structures(Elsevier Ltd., 2016) Taşdemirci, Alper; Güden, Mustafa; Kara, Ali; Taşdemirci, Alper; Turan, Kıvanç; Kara, Ali; Şahin, Selim; Güden, Mustafa; 03.10. Department of Mechanical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of TechnologyThe effect of heat treatment on the dynamic crushing and energy absorption behavior of combined geometry shell cores (hemisphere and cylinder) of sandwich structures were investigated both experimentally and numerically. The applied heat treatment on the combined geometry shell cores relieved the stress caused by deep drawing, diminishing the peak transmitted forces. The verified numerical models of the as-received and heat-treated combined geometry shells were used to model blast loading of various sandwich configurations and the additional sandwich configurations of reversing the cylindrical side of the cores to the impacted side. Both the applied heat-treatment and the reversing process decreased the magnitude of the force transmitted to the protected structure. The applied heat treatment increased the arrival time of blast force wave to the protected structure, while the reversing resulted in opposite.
