WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection

Permanent URI for this collectionhttps://hdl.handle.net/11147/7150

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Author: search.filters.author.Güden, MustafaWoS Q: search.filters.wosQuartile.Q4

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  • Article
    Citation - WoS: 2
    The Effect of the Temperature of Heat Treatment Process and the Concentration and Duration of Acid Leaching on the Size and Crystallinity of Nano-Silica Powders Formed by the Dissociation of Natural Diatom Frustule
    (American Scientific Publishers, 2022) Ülker, Sevkan; Güden, Mustafa
    The present study focused on the processing of nano-silica powders in varying sizes and crystallinities through IP: 846247.10 On: Wed, 14 Dec 2022 07:29:25 heat treatment (900-1200 degrees C), hydrofluoric acid leaching (1-7 N), and ball milling (1 h, 500 rpm) of natural Copyright American Scentfic P blishers diatom frustules. The starting natural frustules were determined to be composed of amorphous silica (88%) Delivered by Ingenta and quartz. The partially ordered crystalline low-quartz and or precursor to low-cristobalite started to form at-900 degrees C. As the heat treatment temperature increased, the crystallinity of the frustules increased from 9.3% at 25 degrees C to 46% at 1200 degrees C. Applying a ball milling reduced the mean particle sizes of the as-received and heat-treated frustules from 15.6-13.7 mu m to 7.2-6.7 mu m, respectively. Acid leaching of the as-received and heat-treated frustules resulted in a further increase in the crystallinity. Furthermore, a ball milling applied after an acid leaching was very effective in reducing the particle size of the as-received and heat-treated frustules. The mean particle size of the acid-leached frustules decreased to 774-547 nm with a crystallinity varying between 12 and 48% after ball milling. A partially dissolved amorphous phase was observed in between crystalline silica grains after acid leaching, which resulted in a rapid fracture/separation of the frustules in ball milling.
  • Article
    Transdiscal Screw Fixation in L5-S1 Spondylolysis: a Biomechanical Study Transdiscal Screw Fixation in L5-51 Spondylolysis
    (Bayrakol Medical Publishing, 2021) Aydın, Murat; Bulut, Tuğrul; Güden, Mustafa; Erel, Nuri
    Aim: This study aimed to investigate whether the L5-S1 transdiscal screw fixation is biomechanically sufficient against axial loads and the resulting shear forces. Material and Methods: Eighteen fresh calf spines under 1 year of age were used in this study. Two randomly selected spines were used as test materials. The inferior facet and ligamentum flavum were removed in 7 randomly selected spines. In these spines (transdiscal screw group), two transdiscal screws were placed bilaterally between 15 and S1. Tests were performed on the remaining 9 spines, while the spines were initially intact (intact group) and after creating a listhesis model (injury group). The extent of displacement occurring as a result of axial loading was noted in all groups in order to calculate the load-displacement curves. Results: The mean displacement as a result of successive axial loadings of 5000 N was as follows: 3 mm (range: 2.4 - 4 mm) in the intact group, 3.5 mm (range: 3 - 4.5 mm) in the transdiscal screw group and 4.5 mm (range: 3.9 - 5 mm) In the group with injury. The difference was statistically significant (p<0.05). None of the samples exhibited broken screws, screw deformation or dislocation, even in failure tests, in the transdiscal screw group. Discussion: These findings have shown that transdiscal screw fixation can be biomechanically sufficient against the shear forces occurring as a result of axial loading. We believe that this technique can be a good alternative as a fixation method for the L5-S1 spondylolisthesis.