WoS İndeksli Yayınlar Koleksiyonu / WoS Indexed Publications Collection
Permanent URI for this collectionhttps://hdl.handle.net/11147/7150
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Conference Object Nanoscale Surface Modification of Ultrahigh Molecular Weight Polyethylene (UHMWPE) Samples With the W Plus C Ion Implantation(Materials Research Soc, 2007) Tıhmınlıoğlu, Funda; Oztarhan, A.; Tihminlioglu, F.; Kaya, N.; Budak, S.; Chhay, B.; Ila, D.; 03.02. Department of Chemical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of TechnologyIn this work, Ultra High Molecular Weight Poly Ethylene (UHMWPE) samples Were implanted by W + C ions using Metal-Vapour Vacuum Arc (MEVVA) ion implantation system with a fluence of 10(17) ion/cm(2) and extraction voltage of 30 kV. Samples were characterized with Raman Spectra, ATR-FTIR, UV-VIS-NlR Spectrum and RBS. Surface morphology of implanted and unimplanted samples were examined in nanoscale with AFM.Conference Object Citation - WoS: 16Thermal Characterization of Ag and Ag Plus N Ion Implanted Ultra-High Molecular Weight Polyethylene (uhmwpe)(Elsevier Ltd., 2007) Urkaç, Emel Sokullu; Tıhmınlıoğlu, Funda; Oztarhan, A.; Tıhmınlıoğlu, Funda; Kaya, N.; Ila, D.; Muntele, C.; Tek, Z.; 03.02. Department of Chemical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of TechnologyMost of total hip joints are composed of ultra-high molecular weight polyethylene (UHMWPE). However, as ultra-high molecular weight polyethylene is too stable in a body, wear debris may accumulate and cause biological response such as bone absorption and loosening of prosthesis. In this study, ultra-high molecular weight polyethylene samples were Ag and Ag + N hybrid ion implanted by using MEVVA ion implantation technique to improve its surface properties. Samples were implanted with a fluence of 10(17) ion/cm(2) and extraction voltage of 30 kV. Implanted and unimplanted samples were investigated by thermo-gravimetry analysis (TGA), differential scanning calorimetry (DSC), X-ray diffraction (XRD) analysis, scanning electron microscopy (SEM), optical microscopy (OM) and contact Angle measurement. Thermal characterization results showed that the ion bombardment induced an increase in the % crystallinity, onset and termination degradation temperatures of UHMWPE. (c) 2007 Elsevier B.V. All rights reserved.Article Citation - WoS: 8Citation - Scopus: 9Polymeric Thermal Analysis of C+h and C+h+ar Ion Implanted Uhmwpe Samples(Elsevier Ltd., 2007) Kaya, N.; Tıhmınlıoğlu, Funda; Öztarhan, Ahmet M.; Urkaç, Emel Sokullu; Ila, D.; Budak, S.; Oks, E.; Tıhmınlıoğlu, Funda; Muntele, C.; 03.02. Department of Chemical Engineering; 03. Faculty of Engineering; 01. Izmir Institute of TechnologyChemical surface characterization of C + H hybrid ion implanted UHMWPE samples were carried out using DSC (differential scanning calorimeter) and TGA (thermal gravimetric analysis) techniques. Samples were implanted with a fluence of 10(17) ion/cm(2) and an extraction voltage of 30 kV. The study of TGA and DSC curves showed that: (1) Polymeric decomposition temperature increased, (2) T-m, Delta C-p and Delta H-m values changed while Delta C-p and Delta H-m increased. T-g value could not be measured, because of some experimental limitations. However, the increase in Delta H-m values showed that T-g values increased, (3) the branch density which indicated the increase in number of cross-link (M-c) decreased in ion implanted samples and (4) increase in Delta H-m values indicated increase in crystallinity of implanted surface of UHMWPE samples.
