Phd Degree / Doktora
Permanent URI for this collectionhttps://hdl.handle.net/11147/2869
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Doctoral Thesis Designing Composite-Based Cylindrical Structures and Manufacturing Composite Prototypes by Filament Winding Method(01. Izmir Institute of Technology, 2024) Martin, Seçkin; Tanoğlu, MetinThis study reports the design, finite element modeling, optimization, fabrication and testing of relatively thick (radius/thickness ~ 7) and long carbon fiber reinforced polymers produced by filament winding against buckling damage under axial loading. The optimum winding angle and stacking sequence against Linear (Eigenvalue) buckling were determined in accordance with the predetermined design requirements utilizing genetic algorithm (GA) optimization via MATLAB. During the optimization process, the critical buckling load factor (λcr) was assigned as objective function, design constraints were natural frequency (fn) and angle of twist (Φ), and ply angles were considered to be variable and restricted with 20 to 87-degree continuous fiber angles in the laminate sequences. As a consequence of the test results, λcr of the proposed optimum model was found to be 3.2 times better than the reference model and both the analytical and finite element model satisfactorily predicted the critical buckling load for all CFRP rods consistent with the test results. The critical buckling loads calculated by applying a KDF of 0.95 for the finite element model and a KDF of 0.9 for the analytical solution were found to be reasonably appropriate for use in the preliminary design input. Additionally, results showed that a higher axial to the circumferential ratio of axial and bending stiffness (A11/A22, D11/D22) promises better buckling performance than other possible candidates. Finally, the microstructures of the produced rods were examined and the fiber volume ratios were calculated by means of chemical characterization.Doctoral Thesis Desing and Production of Light-Weight Pressure Resistant Composite Tank Materials and Systems for Hydrogen Storage(Izmir Institute of Technology, 2020) Kartav, Osman; Tanoğlu, MetinThis thesis focuses on the development of high-pressure resistant composite tanks for hydrogen storage. For this aim, composite tanks with aluminum liners were designed and manufactured by filament winding technique with various lay-up configurations and tested. The main objective of this study was to develop composite tanks with 700 bar working pressure and 1400 bar burst pressure. Furthermore, composite doily layers were incorporated into the filament winding technique and inserted at the front and end dome sections of the composite tanks to improve the burst pressure performance of the composite tanks and to develop the manufacturing process. Before the manufacturing process, the winding simulations were completed using CADWINDTM CAM software. The manufactured composite tanks were hydrostatically loaded with increasing internal pressure up to the burst pressure. During loading, the deformations over the composite tanks and liners were measured locally using strain gauges. Besides, composite plates were manufactured by filament winding technique to determine the mechanical and the thermo-mechanical properties, and the fiber mass fractions of composite sections were determined. Additionally, a preliminary study was carried out to investigate the effect of hybrid fiber usage on the burst pressure performance of steel liner based composite tanks. The effect of filament winding parameters on the burst pressure performance of composite tanks was investigated experimentally. The aimed burst pressure value of more than 1400 bar was obtained in this study for aluminum liner-based carbon fiber reinforced composite tanks. Also, a desired safe burst mode that is expected to occur in the mid-region of the composite tanks was successfully obtained. This study may be useful for the development of composite tanks for high-pressure hydrogen storage especially for the automotive industry and can be helpful to decrease the usage of fossil fuels.Doctoral Thesis Development of Multi and Double Walled Carbon Nanotubes (cnts) / Vinylester Nanocomposites(Izmir Institute of Technology, 2008) Seyhan, Abdullah Tuğrul; Tanoğlu, MetinThis study focuses on development and characterization of thermosetting resin based nanocomposites containing multi and double walled carbon nanotubes with and without amine functional groups (MWCNT, DWCNTs, MWCNT-NH2 and DWCNTNH2).A novel 3-roll milling technique was conducted to prepare the resin suspensions with carbon nanotubes (CNTs). Rheological measurements performed on the resin suspensions showed that addition of very low contents (0.05, 0.1 and 0.3 wt. %) of MWCNTs and MWCNT-NH2 affected the flow characteristic of the resin, significantly.Further, the curing behavior of a vinylester-polyester hybrid resin suspensions containing 0.3 wt % of MWCNTs and MWCNT-NH2 was intensively studied. It was found that regardless of amine groups, presence of CNTs affected the polymerization of the hybrid matrix resin. Final individual fractional conversion rates of styrene and vinylester monomers were found to be vastly dependent on the type of CNTs. Glass transition temperature (Tg) values of the nanocomposites with MWCNTs and MWCNTNH2 were found to increase with filler content. Moreover, nanocomposites containing MWCNTs and MWCNT-NH2 were found to possess higher tensile strength, elastic modulus as well as fracture toughness and fracture energy as compared to the neat hybrid resin. On the other hand, electrical properties of the nanocomposites were also investigated and it was found that nanocomposites with MWCNTs exhibited the lowest percolation threshold value. In addition, nanocomposites with amino functionalized CNTs were found to exhibit lower electrical conductivity as compared to those with untreated CNTs. Nanocomposites with AC electric field induced aligned CNTs were also prepared. Finally, based on the findings obtained for CNT/ resin suspensions, as a case study, electrically conductive glass fiber reinforced composite laminates were successfully produced, using the CNT modified resin suspensions as matrix material, via Vacuum Assisted Resin Transfer Molding (VARTM) and Resin Transfer Molding (RTM) methods.