Phd Degree / Doktora

Permanent URI for this collectionhttps://hdl.handle.net/11147/2869

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Publisher: search.filters.publisher.01. Izmir Institute of TechnologySubject: search.filters.subject.Composite materials

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Now showing 1 - 4 of 4
  • Doctoral Thesis
    Experimental and Numerical Investigation of the Impact Resistance and Impact Damage Tolerance of a Carbon Fiber Reinforced Thermoplastic Polyphenylene Sulfide (pps) Matrix Composite
    (01. Izmir Institute of Technology, 2024) Seven, Semih Berk; Güden, Mustafa; Taşdemirci, Alper
    The impact resistance and impact damage tolerance of an aerospace grade high performance 5 Harness Satin woven fabric carbon fiber reinforced/polyphenylene sulfide matrix (CF/PPS) thermoplastic composite were investigated experimentally and numerically. The numerical modeling was performed using the experimentally determined parameters of material model MAT-58 and Hashin failure criteria in LS-DYNA using the single shell and stacked shell models. The numerical models of the low velocity impact (LVI) tests showed good correlations with the experimental tests while the stacked shell model showed nearer results with the experimental tests. The stacked shell model also estimated the LVI test delamination areas, which were comparable with the experimental damage areas. The LVI tested coupons were further subjected to the compression after impact (CAI) tests in order to determine the damage tolerance of CF/PPS composite. The CAI tests were modeled using the single shell model. The numerical models of the CAI tests showed very similar trends with the experimental CAI tests. The trends were shown to be more converging in the specimens tested at 3 m/s and above in the LVI tests. Lastly, three high velocity impact (HVI) tests were performed at around 100 m/s. The failure mode of the HVI tests was shown to be very different from that of the LVI tests. The long longitudinal and transverse cracks were formed in the HVI tests. The delamination damage in the HVI tests determined using the stacked shell model was found to be more comparable with the experimental delamination damage determined by the C-Scan.
  • Doctoral Thesis
    Designing Composite-Based Cylindrical Structures and Manufacturing Composite Prototypes by Filament Winding Method
    (01. Izmir Institute of Technology, 2024) Martin, Seçkin; Tanoğlu, Metin
    This study reports the design, finite element modeling, optimization, fabrication and testing of relatively thick (radius/thickness ~ 7) and long carbon fiber reinforced polymers produced by filament winding against buckling damage under axial loading. The optimum winding angle and stacking sequence against Linear (Eigenvalue) buckling were determined in accordance with the predetermined design requirements utilizing genetic algorithm (GA) optimization via MATLAB. During the optimization process, the critical buckling load factor (λcr) was assigned as objective function, design constraints were natural frequency (fn) and angle of twist (Φ), and ply angles were considered to be variable and restricted with 20 to 87-degree continuous fiber angles in the laminate sequences. As a consequence of the test results, λcr of the proposed optimum model was found to be 3.2 times better than the reference model and both the analytical and finite element model satisfactorily predicted the critical buckling load for all CFRP rods consistent with the test results. The critical buckling loads calculated by applying a KDF of 0.95 for the finite element model and a KDF of 0.9 for the analytical solution were found to be reasonably appropriate for use in the preliminary design input. Additionally, results showed that a higher axial to the circumferential ratio of axial and bending stiffness (A11/A22, D11/D22) promises better buckling performance than other possible candidates. Finally, the microstructures of the produced rods were examined and the fiber volume ratios were calculated by means of chemical characterization.
  • Doctoral Thesis
    Advanced Material Characterization and Modeling the Foreign Body Impact Damage Initiation and Progression of a Laminated Carbon Composite
    (01. Izmir Institute of Technology, 2023) Bayhan, Mesut; Taşdemirci, Alper; Güden, Mustafa
    The coupon level composite sample tests and the accompanying numerical models were carried out to predict the response of woven carbon fiber composite structures against impact. The numerical models of the coupon-level tests were implemented in LSDYNA software using the MAT_162 and MAT_58 composite material models. The results obtained by both quasi-static and dynamic tests were used to determine their constants. In addition to the tests that were used for the determination and calibration of the material model parameters, separate tests and their models were performed for the validation, including punch shear tests and low-velocity impact tests. It could be said that the material models examined were considered comprehensive and precise as the experimental results were well predicted by the numerical models. Also, the rate sensitivity of the woven carbon composite in the in-plane and thickness directions was investigated experimentally and numerically. In the tests, the DIC method was employed in the determination of the displacement and strain of the specimen. Based on the results obtained, it was concluded that the in-plane tensile properties are rate insensitive. Besides, the simulations of the component level tests, such as bird strike and drone impact, were established to investigate the damage initiation and propagation within the composite. It was found that the drone impact results in more severe damage compared to the bird impact. It is worth noting that the development of such precise composite material models to simulate dynamic loadings will definitely shorten the time between the beginning of designing and the component testing.
  • Doctoral Thesis
    Removal of Dyes and Antibiotics by Adsorption and Photocatalytic Degradation Using Zn-Based Composites
    (01. Izmir Institute of Technology, 2023) Saygı, Gizem; Çakıcıoğlu Özkan, Seher Fehime
    In this study, the ZIF-8 was synthesized and immobilized on the clinoptilolite surface (ZIF8@CLN) and doped with Ag nanoparticles, forming the Ag-ZIF8 and Ag-ZIF8@CLN composite materials. The characterization results indicated that the ZIF-8 was well-deposited on the clinoptilolite surface and doped successfully with Ag nanoparticles. The adsorption and photocatalytic activity of these adsorbents/catalysts were evaluated by the removal of the organic pollutants such as dyes and antibiotics. The target dyes were cationic Methylene blue (MB), anionic Methyl orange (MO) and Congo red (CR), and zwitterionic Rhodamine B (RhB). The target antibiotic was tetracycline (TC). The influence of various parameters on removal was investigated using different initial pH, photocatalyst amount, pollutant concentrations and ionic strength. The results showed that ZIF-8 and ZIF-8@CLN are excellent adsorbents. However, the photocatalytic activity of Ag-ZIF8 and especially Ag-ZIF8@CLN composites were much better than ZIF-8 and ZIF-8@CLN for degradation of all dyes. The Ag-ZIF8 and Ag-ZIF8@CLN composite catalysts exhibited more than 90% removal capacity under UV irradiation for 120 min with the dye concentration of 25 mg L-1 at the optimum pHs of each dye. The enhanced adsorption and photocatalytic performance of the composite photocatalysts was attributed to the synergistic effect between the ZIF-8, CLN and Ag. The adsorption data were evaluated by considering adsorption isotherms, kinetics and thermodynamics using target dyes and antibiotics. Proposed photodegradation mechanism of the dyes over Ag-ZIF8@CLN was explained detailed. This work introduced the ZIF-8-based composite photocatalysts with high efficiency, and may provide to prefer these catalysts in photocatalytic field.