Phd Degree / Doktora

Permanent URI for this collectionhttps://hdl.handle.net/11147/2869

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  • Doctoral Thesis
    Performance Improvement of Composite Materials Used as Hydrogen Storage Tanks by Microstructural Modifications
    (Izmir Institute of Technology, 2020) Ay, Zeynep; Tanoğlu, Metin
    The goal of this Ph.D. thesis is to improve the performance of the cylindrical composites manufactured by filament winding method by using the toughened matrix resin with nano-sized filler (noncovalently functionalized with ethoxylated alcohol chemical-vapor-deposition-grown SWCNTs). The effect of SWCNT concentration on the mechanical performance of these composites was investigated and discussed. One of the main focus of this thesis is to examine the effect of nano-sized filler type and filler concentration on the performance of the epoxy-based composites. For this purpose, epoxy-based nanocomposites with different nano-sized filler types (SWCNT, TEGO, and HNT) at varying concentrations were developed by a calendaring (3-roll-mill) method. A series of mechanical tests were performed for reference composite and developed nanocomposites. The scanning electron microscopy (SEM) was used to reveal the morphology and toughening mechanisms by examining the fractured surface of nanocomposites. The rheological behaviors and contact angle measurements with glass fiber of the selected filler (SWCNT) incorporated epoxy suspensions were investigated to determine the suitability of suspensions for the filament winding process. The reference and SWCNT modified glass fiber (GF)-based cylindrical fiber-reinforced polymeric composites (CFRPCs) with an inner diameter of 60 and 275 mm were manufactured by the filament winding method. The split-disk and three-point bending tests were performed for GF-based CFRPCs. The double cantilever beam (DCB) test was also carried out for the reference and SWCNT modified GF-based CFRPCs to investigate the effect of SWCNT existence on the interlaminar fracture toughness of CFRPCs. The fractured surfaces after the DCB test were analyzed under the SEM to comprehend the toughening mechanisms, and micro-and nano-sized filler morphologies. Consequently, it was revealed that blending and hence toughening the epoxy resin with SWCNT improves the interlaminar properties of the GF-based composites.
  • Doctoral Thesis
    The Penetration Behavior of Repeated Hemisphere Core Sandwich Structures: an Experimental and Numerical Study
    (Izmir Institute of Technology, 2018) Turan, Ali Kıvanç; Taşdemirci, Alper; Güden, Mustafa
    In this study, penetration behavior of novel core structure consisting hemispherical and cylindrical parts was investigated. Core units were manufactured with deep drawing method in two thicknesses to have monolithic form without any sort of assembly method or element. Produced specimens were then subjected to penetration tests at low and intermediate velocities against blunt, conical and hemispherical tipped indenters using special fixtures and apparatuses on conventional testing equipment. Effect of heat treatment on penetration behavior was investigated to observe whether residual stresses arise from manufacturing process changes the penetration behavior. Confinement effects were studied experimentally with a special fixture, allowing tested specimen to be radially confined with other core units as in an armor structure. Finally, experimental work was finished by conducting a case study where core units were subjected to spherical projectile impact up to impact velocities of 180 m.s-1 in a composite sandwich structure. Results show that each indenter geometry showed unique deformation characteristics in testing of both core units and both of the core geometries were able to hold a steel spherical projectile with mass of 110 g without full perforation at impact velocity of 180 m.s-1. Details of experimental results were presented in each chapter. Study also included modeling parts where core units were numerically produced with residual stresses and strains and good correlation was noted where thickness was compared with actual measurements on core units. Test conducted on single core structure in as-received and heat-treated condition were also repeated in numerical environment, where numerical study exhibited good correlation on both forcedisplacement curves and deformation of core units with tests. Correlation achieved with experimental study has led into further investigations of strain rate and micro-inertia where behavior of core units was studied at numerical impact velocities of 300 m.s-1. Results show that both strain rate and micro-inertia increase the local maximums and average of force levels. Effect of strain rate and micro-inertia is clearly distinguished for a threshold displacement level where micro-inertia is further dominant on behavior.
  • Doctoral Thesis
    Experimental and Numerical Evaluation of the Blast-Like Loading of Fiber Reinforced Polymer Composites and Aluminum Corrugated Core Composite Sandwiches Through Projectile Impact Testing Using Aluminum Corrugated Projectiles
    (Izmir Institute of Technology, 2015) Odacı, İsmet Kutlay; Güden, Mustafa; Taşdemirci, Alper
    This thesis develops and validates a laboratory scale blast-like testing method that can simulate explosive blast tests in air and under water without using explosives. The study has mainly focused on the shock loading potential of 1050 H14 trapezoidal corrugated core aluminium sandwich structures on E-glass/polyester composite plates and corrugated core composite sandwich structures experimentally, numerically and analytically. The composite plates were modelled using MAT_162 material model in LS-DYNA finite element code. Quasi-static and high strain rate tests were performed to determine the material model parameters of composite and corrugated structure. The resultant parameters were calibrated and validated by comparing the numerical results with the experimental results. The planar shock wave formation and propagation in corrugated core sandwich structures were shown experimentally using a direct impact Split Hopkinson Pressure Bar test set-up. Rigid-perfectly-plastic-locking material model and Hugoniot jump relations revealed the shock loading potential of the tested corrugated core sandwich structures. The shock loading response of composite plates and sandwich structures were investigated by firing the corrugated sandwich projectiles on the targets. These impact tests were also simulated numerically and an analytic model was used to predict the plate deflections. The experimentally, numerically and analytically determined back face deflections were compared with the deflections of the Conwep blast simulations in LS-DYNA. The results have shown that the corrugated core sandwich structures can generate shock loading as in the explosive blast tests and can be used to produce shock loads in laboratory scale experiments.