Phd Degree / Doktora
Permanent URI for this collectionhttps://hdl.handle.net/11147/2869
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Doctoral Thesis Experimental and Numerical Investigation of the Impact Resistance and Impact Damage Tolerance of a Carbon Fiber Reinforced Thermoplastic Polyphenylene Sulfide (pps) Matrix Composite(01. Izmir Institute of Technology, 2024) Seven, Semih Berk; Güden, Mustafa; Taşdemirci, AlperThe impact resistance and impact damage tolerance of an aerospace grade high performance 5 Harness Satin woven fabric carbon fiber reinforced/polyphenylene sulfide matrix (CF/PPS) thermoplastic composite were investigated experimentally and numerically. The numerical modeling was performed using the experimentally determined parameters of material model MAT-58 and Hashin failure criteria in LS-DYNA using the single shell and stacked shell models. The numerical models of the low velocity impact (LVI) tests showed good correlations with the experimental tests while the stacked shell model showed nearer results with the experimental tests. The stacked shell model also estimated the LVI test delamination areas, which were comparable with the experimental damage areas. The LVI tested coupons were further subjected to the compression after impact (CAI) tests in order to determine the damage tolerance of CF/PPS composite. The CAI tests were modeled using the single shell model. The numerical models of the CAI tests showed very similar trends with the experimental CAI tests. The trends were shown to be more converging in the specimens tested at 3 m/s and above in the LVI tests. Lastly, three high velocity impact (HVI) tests were performed at around 100 m/s. The failure mode of the HVI tests was shown to be very different from that of the LVI tests. The long longitudinal and transverse cracks were formed in the HVI tests. The delamination damage in the HVI tests determined using the stacked shell model was found to be more comparable with the experimental delamination damage determined by the C-Scan.Doctoral Thesis Designing Composite-Based Cylindrical Structures and Manufacturing Composite Prototypes by Filament Winding Method(01. Izmir Institute of Technology, 2024) Martin, Seçkin; Tanoğlu, MetinThis study reports the design, finite element modeling, optimization, fabrication and testing of relatively thick (radius/thickness ~ 7) and long carbon fiber reinforced polymers produced by filament winding against buckling damage under axial loading. The optimum winding angle and stacking sequence against Linear (Eigenvalue) buckling were determined in accordance with the predetermined design requirements utilizing genetic algorithm (GA) optimization via MATLAB. During the optimization process, the critical buckling load factor (λcr) was assigned as objective function, design constraints were natural frequency (fn) and angle of twist (Φ), and ply angles were considered to be variable and restricted with 20 to 87-degree continuous fiber angles in the laminate sequences. As a consequence of the test results, λcr of the proposed optimum model was found to be 3.2 times better than the reference model and both the analytical and finite element model satisfactorily predicted the critical buckling load for all CFRP rods consistent with the test results. The critical buckling loads calculated by applying a KDF of 0.95 for the finite element model and a KDF of 0.9 for the analytical solution were found to be reasonably appropriate for use in the preliminary design input. Additionally, results showed that a higher axial to the circumferential ratio of axial and bending stiffness (A11/A22, D11/D22) promises better buckling performance than other possible candidates. Finally, the microstructures of the produced rods were examined and the fiber volume ratios were calculated by means of chemical characterization.Doctoral Thesis Advanced Material Characterization and Modeling the Foreign Body Impact Damage Initiation and Progression of a Laminated Carbon Composite(01. Izmir Institute of Technology, 2023) Bayhan, Mesut; Taşdemirci, Alper; Güden, MustafaThe coupon level composite sample tests and the accompanying numerical models were carried out to predict the response of woven carbon fiber composite structures against impact. The numerical models of the coupon-level tests were implemented in LSDYNA software using the MAT_162 and MAT_58 composite material models. The results obtained by both quasi-static and dynamic tests were used to determine their constants. In addition to the tests that were used for the determination and calibration of the material model parameters, separate tests and their models were performed for the validation, including punch shear tests and low-velocity impact tests. It could be said that the material models examined were considered comprehensive and precise as the experimental results were well predicted by the numerical models. Also, the rate sensitivity of the woven carbon composite in the in-plane and thickness directions was investigated experimentally and numerically. In the tests, the DIC method was employed in the determination of the displacement and strain of the specimen. Based on the results obtained, it was concluded that the in-plane tensile properties are rate insensitive. Besides, the simulations of the component level tests, such as bird strike and drone impact, were established to investigate the damage initiation and propagation within the composite. It was found that the drone impact results in more severe damage compared to the bird impact. It is worth noting that the development of such precise composite material models to simulate dynamic loadings will definitely shorten the time between the beginning of designing and the component testing.Doctoral Thesis Removal of Dyes and Antibiotics by Adsorption and Photocatalytic Degradation Using Zn-Based Composites(01. Izmir Institute of Technology, 2023) Saygı, Gizem; Çakıcıoğlu Özkan, Seher FehimeIn this study, the ZIF-8 was synthesized and immobilized on the clinoptilolite surface (ZIF8@CLN) and doped with Ag nanoparticles, forming the Ag-ZIF8 and Ag-ZIF8@CLN composite materials. The characterization results indicated that the ZIF-8 was well-deposited on the clinoptilolite surface and doped successfully with Ag nanoparticles. The adsorption and photocatalytic activity of these adsorbents/catalysts were evaluated by the removal of the organic pollutants such as dyes and antibiotics. The target dyes were cationic Methylene blue (MB), anionic Methyl orange (MO) and Congo red (CR), and zwitterionic Rhodamine B (RhB). The target antibiotic was tetracycline (TC). The influence of various parameters on removal was investigated using different initial pH, photocatalyst amount, pollutant concentrations and ionic strength. The results showed that ZIF-8 and ZIF-8@CLN are excellent adsorbents. However, the photocatalytic activity of Ag-ZIF8 and especially Ag-ZIF8@CLN composites were much better than ZIF-8 and ZIF-8@CLN for degradation of all dyes. The Ag-ZIF8 and Ag-ZIF8@CLN composite catalysts exhibited more than 90% removal capacity under UV irradiation for 120 min with the dye concentration of 25 mg L-1 at the optimum pHs of each dye. The enhanced adsorption and photocatalytic performance of the composite photocatalysts was attributed to the synergistic effect between the ZIF-8, CLN and Ag. The adsorption data were evaluated by considering adsorption isotherms, kinetics and thermodynamics using target dyes and antibiotics. Proposed photodegradation mechanism of the dyes over Ag-ZIF8@CLN was explained detailed. This work introduced the ZIF-8-based composite photocatalysts with high efficiency, and may provide to prefer these catalysts in photocatalytic field.Doctoral Thesis Desing and Production of Light-Weight Pressure Resistant Composite Tank Materials and Systems for Hydrogen Storage(Izmir Institute of Technology, 2020) Kartav, Osman; Tanoğlu, MetinThis thesis focuses on the development of high-pressure resistant composite tanks for hydrogen storage. For this aim, composite tanks with aluminum liners were designed and manufactured by filament winding technique with various lay-up configurations and tested. The main objective of this study was to develop composite tanks with 700 bar working pressure and 1400 bar burst pressure. Furthermore, composite doily layers were incorporated into the filament winding technique and inserted at the front and end dome sections of the composite tanks to improve the burst pressure performance of the composite tanks and to develop the manufacturing process. Before the manufacturing process, the winding simulations were completed using CADWINDTM CAM software. The manufactured composite tanks were hydrostatically loaded with increasing internal pressure up to the burst pressure. During loading, the deformations over the composite tanks and liners were measured locally using strain gauges. Besides, composite plates were manufactured by filament winding technique to determine the mechanical and the thermo-mechanical properties, and the fiber mass fractions of composite sections were determined. Additionally, a preliminary study was carried out to investigate the effect of hybrid fiber usage on the burst pressure performance of steel liner based composite tanks. The effect of filament winding parameters on the burst pressure performance of composite tanks was investigated experimentally. The aimed burst pressure value of more than 1400 bar was obtained in this study for aluminum liner-based carbon fiber reinforced composite tanks. Also, a desired safe burst mode that is expected to occur in the mid-region of the composite tanks was successfully obtained. This study may be useful for the development of composite tanks for high-pressure hydrogen storage especially for the automotive industry and can be helpful to decrease the usage of fossil fuels.Doctoral Thesis Experimental and Numerical Evaluation of the Blast-Like Loading of Fiber Reinforced Polymer Composites and Aluminum Corrugated Core Composite Sandwiches Through Projectile Impact Testing Using Aluminum Corrugated Projectiles(Izmir Institute of Technology, 2015) Odacı, İsmet Kutlay; Güden, Mustafa; Taşdemirci, AlperThis thesis develops and validates a laboratory scale blast-like testing method that can simulate explosive blast tests in air and under water without using explosives. The study has mainly focused on the shock loading potential of 1050 H14 trapezoidal corrugated core aluminium sandwich structures on E-glass/polyester composite plates and corrugated core composite sandwich structures experimentally, numerically and analytically. The composite plates were modelled using MAT_162 material model in LS-DYNA finite element code. Quasi-static and high strain rate tests were performed to determine the material model parameters of composite and corrugated structure. The resultant parameters were calibrated and validated by comparing the numerical results with the experimental results. The planar shock wave formation and propagation in corrugated core sandwich structures were shown experimentally using a direct impact Split Hopkinson Pressure Bar test set-up. Rigid-perfectly-plastic-locking material model and Hugoniot jump relations revealed the shock loading potential of the tested corrugated core sandwich structures. The shock loading response of composite plates and sandwich structures were investigated by firing the corrugated sandwich projectiles on the targets. These impact tests were also simulated numerically and an analytic model was used to predict the plate deflections. The experimentally, numerically and analytically determined back face deflections were compared with the deflections of the Conwep blast simulations in LS-DYNA. The results have shown that the corrugated core sandwich structures can generate shock loading as in the explosive blast tests and can be used to produce shock loads in laboratory scale experiments.Doctoral Thesis Development of Multi and Double Walled Carbon Nanotubes (cnts) / Vinylester Nanocomposites(Izmir Institute of Technology, 2008) Seyhan, Abdullah Tuğrul; Tanoğlu, MetinThis study focuses on development and characterization of thermosetting resin based nanocomposites containing multi and double walled carbon nanotubes with and without amine functional groups (MWCNT, DWCNTs, MWCNT-NH2 and DWCNTNH2).A novel 3-roll milling technique was conducted to prepare the resin suspensions with carbon nanotubes (CNTs). Rheological measurements performed on the resin suspensions showed that addition of very low contents (0.05, 0.1 and 0.3 wt. %) of MWCNTs and MWCNT-NH2 affected the flow characteristic of the resin, significantly.Further, the curing behavior of a vinylester-polyester hybrid resin suspensions containing 0.3 wt % of MWCNTs and MWCNT-NH2 was intensively studied. It was found that regardless of amine groups, presence of CNTs affected the polymerization of the hybrid matrix resin. Final individual fractional conversion rates of styrene and vinylester monomers were found to be vastly dependent on the type of CNTs. Glass transition temperature (Tg) values of the nanocomposites with MWCNTs and MWCNTNH2 were found to increase with filler content. Moreover, nanocomposites containing MWCNTs and MWCNT-NH2 were found to possess higher tensile strength, elastic modulus as well as fracture toughness and fracture energy as compared to the neat hybrid resin. On the other hand, electrical properties of the nanocomposites were also investigated and it was found that nanocomposites with MWCNTs exhibited the lowest percolation threshold value. In addition, nanocomposites with amino functionalized CNTs were found to exhibit lower electrical conductivity as compared to those with untreated CNTs. Nanocomposites with AC electric field induced aligned CNTs were also prepared. Finally, based on the findings obtained for CNT/ resin suspensions, as a case study, electrically conductive glass fiber reinforced composite laminates were successfully produced, using the CNT modified resin suspensions as matrix material, via Vacuum Assisted Resin Transfer Molding (VARTM) and Resin Transfer Molding (RTM) methods.Doctoral Thesis Design of Dimensionally-Stable Laminated Somposites Subjected To Hygro-Thermo Loading by Stochastic Optimization Methods(Izmir Institute of Technology, 2011) Aydın, Levent; Artem, Hatice SeçilThe materials used in aerospace structures such as antenna, satellites and missiles should have such features as low density, high stiffness, low coefficients of thermal and moisture expansions simultaneously. Fiber reinforced polymer composite materials can satisfy these requirements with an appropriate stacking sequence using optimization methods and hence dimensionally stable composites are obtained. In this thesis, two different materials carbon/epoxy and E-glass/epoxy composites are considered. Both materials have been used for optimization, stress and failure analysis. However, only for E-glass/epoxy, experimental studies have been performed including determination of stiffness, strength characteristics, Poisson's ratio, fiber volume fraction, glass transition temperature (Tg) and coefficient of thermal expansion (CTE). The objective of optimization part is to design the stacking sequence of the carbon/epoxy and E-glass/epoxy laminated composites having low CTE and high elastic moduli. In design process, multi-objective genetic algorithm optimization of the carbon/epoxy composite plates are verified by single-objective optimization approach by using the Genetic Algorithm (GA), Generalized Pattern Search (GPS) and Simulated Annealing (SA) algorithms. MATLAB Optimization Toolbox is used to obtain Pareto-optimal designs and global optimum points for different model problems. Stress and strain distributions are presented through the thickness of the laminates subjected to mechanical, thermal, and hygral loadings. Stress analysis results showed that effect of mechanical loads dominate to hygral and thermal loads. All the stochastic search methods carried out in the present thesis have produced almost the same results with different stacking sequences.